(Z)-2-(2-iodoethenyl)-4-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)bromobenzene

Base Information

Chemical Name:(Z)-2-(2-iodoethenyl)-4-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)bromobenzene
CAS No.:960325-72-8
Molecular Formula:C₁₇H₂₂BrIO₅
Molecular Weight:513.167
Hs Code.:

Synonyms:(Z)-2-(2-iodoethenyl)-4-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)bromobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(2-iodoethenyl)-4-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)bromobenzene

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Technology Process of (Z)-2-(2-iodoethenyl)-4-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)bromobenzene

There total 1 articles about (Z)-2-(2-iodoethenyl)-4-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)bromobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 2-bromo-5-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)benzaldehyde

: 3020-28-8
(iodomethyl)triphenylphosphonium iodide

: 960325-72-8
(Z)-2-(2-iodoethenyl)-4-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)bromobenzene

Guidance literature:: (iodomethyl)triphenylphosphonium iodide; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 20 ℃; for 0.0833333h;

2-bromo-5-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)benzaldehyde; In tetrahydrofuran; toluene; at -78 - 20 ℃; for 1.75h; Further stages.;
DOI:10.1002/chem.200700464

Reference yield: 42.0%

: 960325-72-8
(Z)-2-(2-iodoethenyl)-4-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)bromobenzene

: rac-2-[(5-tert-butyldimethylsilyloxymethyl)cyclopent-2-enyl]acetic acid tert-butyl ester

: [2-(Z)-(2-[2-bromo-5-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)phenyl]vinyl)-5-tert-butyldimethylsilyloxymethylcyclopent-3-enyl]acetic acid tert-butyl ester

: {3-(Z)-(2-[2-bromo-5-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)phenyl]vinyl)-5-tert-butyldimethylsilyloxymethylcyclopent-1-enyl}acetic acid tert-butyl ester

Guidance literature:: With tetrabutyl-ammonium chloride; sodium acetate; palladium diacetate; In N,N-dimethyl-formamide; at 20 ℃; for 72h;
DOI:10.1002/chem.200700464

Reference yield: 42.0%

: 960325-72-8
(Z)-2-(2-iodoethenyl)-4-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)bromobenzene

: rac-2-[(5-tert-butyldimethylsilyloxymethyl)cyclopent-2-enyl]acetic acid methyl ester

: [2-(Z)-(2-[2-bromo-5-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)phenyl]vinyl)-5-tert-butyldimethylsilyloxymethylcyclopent-3-enyl]acetic acid methyl ester

: {3-(Z)-(2-[2-bromo-5-(2,3,4-tri-O-methyl-α-L-rhamnopyranosyl)phenyl]vinyl)-5-tert-butyldimethylsilyloxymethylcyclopent-1-enyl}acetic acid methyl ester

Guidance literature:: With tetrabutyl-ammonium chloride; sodium carbonate; palladium diacetate; In N,N-dimethyl-formamide; at 20 ℃; for 72h;
DOI:10.1002/chem.200700464