Technology Process of ar-Pseudotsugonoxide
There total 9 articles about ar-Pseudotsugonoxide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
benzene;
for 2h;
Heating;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 82 percent / p-TosOH / benzene / Heating
2: 70 percent / LiAlH4 / diethyl ether / 2.5 h / Heating
3: 54 percent / pyridinium chlorochromate/NaOAc / CH2Cl2 / 2.5 h / Ambient temperature
4: 1. Mg / 1. THF 2. THF/room temperature/overnight, then 2 h/reflux
5: 77 percent / aq. HCl / acetone / 2 h
6: 1. Mg / 1. Et2O 2. Et2O/room temperature/overnight
7: 50 percent / Jones' reagent / acetone
8: 75 percent / sodium hydride / benzene / 2 h / Heating
With
hydrogenchloride; lithium aluminium tetrahydride; jones' reagent; sodium acetate; sodium hydride; magnesium; pyridinium chlorochromate;
toluene-4-sulfonic acid;
In
diethyl ether; dichloromethane; acetone; benzene;
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 65 percent / NaH / benzene; dimethylformamide / 0.5 h / Heating
2: 82 percent / p-TosOH / benzene / Heating
3: 70 percent / LiAlH4 / diethyl ether / 2.5 h / Heating
4: 54 percent / pyridinium chlorochromate/NaOAc / CH2Cl2 / 2.5 h / Ambient temperature
5: 1. Mg / 1. THF 2. THF/room temperature/overnight, then 2 h/reflux
6: 77 percent / aq. HCl / acetone / 2 h
7: 1. Mg / 1. Et2O 2. Et2O/room temperature/overnight
8: 50 percent / Jones' reagent / acetone
9: 75 percent / sodium hydride / benzene / 2 h / Heating
With
hydrogenchloride; lithium aluminium tetrahydride; jones' reagent; sodium acetate; sodium hydride; magnesium; pyridinium chlorochromate;
toluene-4-sulfonic acid;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone; benzene;
