(Z)-7-Acetoxy-1-<(3-acetoxy-4-methoxyphenyl)methylene>-2-acetyl-6-methoxy-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:(Z)-7-Acetoxy-1-<(3-acetoxy-4-methoxyphenyl)methylene>-2-acetyl-6-methoxy-1,2,3,4-tetrahydroisoquinoline
CAS No.:104621-41-2
Molecular Formula:C₂₄H₂₅NO₇
Molecular Weight:439.465
Hs Code.:

Synonyms:(Z)-7-Acetoxy-1-<(3-acetoxy-4-methoxyphenyl)methylene>-2-acetyl-6-methoxy-1,2,3,4-tetrahydroisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-7-Acetoxy-1-<(3-acetoxy-4-methoxyphenyl)methylene>-2-acetyl-6-methoxy-1,2,3,4-tetrahydroisoquinoline

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Technology Process of (Z)-7-Acetoxy-1-<(3-acetoxy-4-methoxyphenyl)methylene>-2-acetyl-6-methoxy-1,2,3,4-tetrahydroisoquinoline

There total 1 articles about (Z)-7-Acetoxy-1-<(3-acetoxy-4-methoxyphenyl)methylene>-2-acetyl-6-methoxy-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 72258-91-4
1,2-dehydronorreticuline

: 108-24-7
acetic anhydride

: 104621-41-2
(Z)-7-Acetoxy-1-<(3-acetoxy-4-methoxyphenyl)methylene>-2-acetyl-6-methoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With pyridine; at 140 ℃; for 4h;
DOI:10.1021/jo00081a007

Reference yield: 88.0%

: 104621-41-2
(Z)-7-Acetoxy-1-<(3-acetoxy-4-methoxyphenyl)methylene>-2-acetyl-6-methoxy-1,2,3,4-tetrahydroisoquinoline

: (R)-N-acetyl-7-acetoxy-1-(3-acetoxy-4-methoxyphenylmethyl)-6-methoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: In ethanol; dichloromethane;

Reference yield:

: 104621-41-2
(Z)-7-Acetoxy-1-<(3-acetoxy-4-methoxyphenyl)methylene>-2-acetyl-6-methoxy-1,2,3,4-tetrahydroisoquinoline

: Acetic acid (S)-1-(3-acetoxy-4-methoxy-benzyl)-2-acetyl-6-methoxy-1,2,3,4-tetrahydro-isoquinolin-7-yl ester

: (R)-N-acetyl-7-acetoxy-1-(3-acetoxy-4-methoxyphenylmethyl)-6-methoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With hydrogen; (S)-Ru(OAc)₂-BINAP; In ethanol; dichloromethane; at 24 ℃; for 49h; under 3040 Torr; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00081a007