tert-butyl [(Z)-{[3-bromo-4-(bromomethyl)benzyl]amino} {[( tert-butyloxy)carbonyl]amino}methylidene]carbamate

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Chemical Name:tert-butyl [(Z)-{[3-bromo-4-(bromomethyl)benzyl]amino} {[( tert-butyloxy)carbonyl]amino}methylidene]carbamate
CAS No.:1427087-11-3
Molecular Formula:C₁₉H₂₇Br₂N₃O₄
Molecular Weight:521.249
Hs Code.:

Synonyms:tert-butyl [(Z)-{[3-bromo-4-(bromomethyl)benzyl]amino} {[( tert-butyloxy)carbonyl]amino}methylidene]carbamate

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Chemical Property of tert-butyl [(Z)-{[3-bromo-4-(bromomethyl)benzyl]amino} {[( tert-butyloxy)carbonyl]amino}methylidene]carbamate

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Technology Process of tert-butyl [(Z)-{[3-bromo-4-(bromomethyl)benzyl]amino} {[( tert-butyloxy)carbonyl]amino}methylidene]carbamate

There total 6 articles about tert-butyl [(Z)-{[3-bromo-4-(bromomethyl)benzyl]amino} {[( tert-butyloxy)carbonyl]amino}methylidene]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427086-98-3
tert-butyl [(Z)-{[3-bromo-4-(hydroxymethyl)benzyl]amino} {[( tert-butyloxy)carbonyl]amino}methylidene]carbamate

: 1427087-11-3
tert-butyl [(Z)-{[3-bromo-4-(bromomethyl)benzyl]amino} {[( tert-butyloxy)carbonyl]amino}methylidene]carbamate

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 42872-74-2
3-bromo-4-methyl-benzonitrile

: 1427087-11-3
tert-butyl [(Z)-{[3-bromo-4-(bromomethyl)benzyl]amino} {[( tert-butyloxy)carbonyl]amino}methylidene]carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 48 h / Reflux

2: dimethyl sulfoxide / water / 6 h / 120 °C

3: sodium tetrahydroborate; methanol / 0.67 h / 0 °C

4: lithium aluminium tetrahydride / tetrahydrofuran; methanol / 16 h / 0 - 20 °C

5: acetonitrile / 0.5 h / 20 °C

6: carbon tetrabromide; triphenylphosphine / dichloromethane / 2 h / 20 °C

With methanol; sodium tetrahydroborate; N-Bromosuccinimide; lithium aluminium tetrahydride; carbon tetrabromide; dimethyl sulfoxide; triphenylphosphine; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; water; acetonitrile;

Reference yield:

: 1381846-22-5
3-bromo-4-(dibromomethyl)benzonitrile

: 1427087-11-3
tert-butyl [(Z)-{[3-bromo-4-(bromomethyl)benzyl]amino} {[( tert-butyloxy)carbonyl]amino}methylidene]carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: dimethyl sulfoxide / water / 6 h / 120 °C

2: sodium tetrahydroborate; methanol / 0.67 h / 0 °C

3: lithium aluminium tetrahydride / tetrahydrofuran; methanol / 16 h / 0 - 20 °C

4: acetonitrile / 0.5 h / 20 °C

5: carbon tetrabromide; triphenylphosphine / dichloromethane / 2 h / 20 °C

With methanol; sodium tetrahydroborate; lithium aluminium tetrahydride; carbon tetrabromide; dimethyl sulfoxide; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;