2,2'-(5,5'-(5-butyl-4,6-dioxo-5,6-dihydro-4H-thieno[3,4-c]pyrrole-1,3-diyl)bis(thiophene-5,2-diyl))bis(5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

Base Information

Chemical Name:2,2'-(5,5'-(5-butyl-4,6-dioxo-5,6-dihydro-4H-thieno[3,4-c]pyrrole-1,3-diyl)bis(thiophene-5,2-diyl))bis(5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)
CAS No.:1598437-80-9
Molecular Formula:C₄₈H₃₅Cl₂N₃O₆S₅
Molecular Weight:981.058
Hs Code.:

2,2'-(5,5'-(5-butyl-4,6-dioxo-5,6-dihydro-4H-thieno[3,4-c]pyrrole-1,3-diyl)bis(thiophene-5,2-diyl))bis(5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

Synonyms:2,2'-(5,5'-(5-butyl-4,6-dioxo-5,6-dihydro-4H-thieno[3,4-c]pyrrole-1,3-diyl)bis(thiophene-5,2-diyl))bis(5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

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Chemical Property of 2,2'-(5,5'-(5-butyl-4,6-dioxo-5,6-dihydro-4H-thieno[3,4-c]pyrrole-1,3-diyl)bis(thiophene-5,2-diyl))bis(5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

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Technology Process of 2,2'-(5,5'-(5-butyl-4,6-dioxo-5,6-dihydro-4H-thieno[3,4-c]pyrrole-1,3-diyl)bis(thiophene-5,2-diyl))bis(5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

There total 5 articles about 2,2'-(5,5'-(5-butyl-4,6-dioxo-5,6-dihydro-4H-thieno[3,4-c]pyrrole-1,3-diyl)bis(thiophene-5,2-diyl))bis(5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1598437-79-6
2-(5-bromothiophen-2-yl)-5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[ 2,3-c]pyrrole-4,6-dione

: 1428567-53-6
5-butyl-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione

: 1598437-80-9
2,2'-(5,5'-(5-butyl-4,6-dioxo-5,6-dihydro-4H-thieno[3,4-c]pyrrole-1,3-diyl)bis(thiophene-5,2-diyl))bis(5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

Guidance literature:: With palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; In toluene; for 5h; Reflux;

Reference yield:

: 1598437-76-3
5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione

: 1598437-80-9
2,2'-(5,5'-(5-butyl-4,6-dioxo-5,6-dihydro-4H-thieno[3,4-c]pyrrole-1,3-diyl)bis(thiophene-5,2-diyl))bis(5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

Guidance literature:: Multi-step reaction with 3 steps

1: tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; potassium carbonate; palladium diacetate / toluene / 5 h / Reflux

2: sulfuric acid; N-Bromosuccinimide / dichloromethane; acetic acid / 0 - 20 °C / Darkness

3: tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; potassium carbonate; palladium diacetate / toluene / 5 h / Reflux

With N-Bromosuccinimide; sulfuric acid; palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; In dichloromethane; acetic acid; toluene;

Reference yield:

: 1598437-78-5
5-(3-chloro-2,4,6-trimethylphenyl)-2-(thiophen-2-yl)-5H-thieno[2,3-c]pyrrole-4,6-dione

: 1598437-80-9
2,2'-(5,5'-(5-butyl-4,6-dioxo-5,6-dihydro-4H-thieno[3,4-c]pyrrole-1,3-diyl)bis(thiophene-5,2-diyl))bis(5-(3-chloro-2,4,6-trimethylphenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; N-Bromosuccinimide / dichloromethane; acetic acid / 0 - 20 °C / Darkness

2: tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; potassium carbonate; palladium diacetate / toluene / 5 h / Reflux

With N-Bromosuccinimide; sulfuric acid; palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; In dichloromethane; acetic acid; toluene;