1,4,5,8-tetrahydro-1,4:5,8-dimethanoanthracene-9,10-bis(phenylphosphonic acid ester)

Base Information

Chemical Name:1,4,5,8-tetrahydro-1,4:5,8-dimethanoanthracene-9,10-bis(phenylphosphonic acid ester)
CAS No.:848486-27-1
Molecular Formula:C₂₈H₂₄O₆P₂
Molecular Weight:518.442
Hs Code.:

Synonyms:1,4,5,8-tetrahydro-1,4:5,8-dimethanoanthracene-9,10-bis(phenylphosphonic acid ester)

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Chemical Property of 1,4,5,8-tetrahydro-1,4:5,8-dimethanoanthracene-9,10-bis(phenylphosphonic acid ester)

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Technology Process of 1,4,5,8-tetrahydro-1,4:5,8-dimethanoanthracene-9,10-bis(phenylphosphonic acid ester)

There total 3 articles about 1,4,5,8-tetrahydro-1,4:5,8-dimethanoanthracene-9,10-bis(phenylphosphonic acid ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₂₂Cl₂O₄P₂

: 848486-27-1
1,4,5,8-tetrahydro-1,4:5,8-dimethanoanthracene-9,10-bis(phenylphosphonic acid ester)

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; hexane;
DOI:10.1002/chem.200400603

Reference yield:

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 848486-27-1
1,4,5,8-tetrahydro-1,4:5,8-dimethanoanthracene-9,10-bis(phenylphosphonic acid ester)

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 1 h / 0 °C

2: 110 mg / aq. HCl / tetrahydrofuran; hexane

With hydrogenchloride; triethylamine; In tetrahydrofuran; hexane;
DOI:10.1002/chem.200400603

Reference yield:

: 119363-89-2
syn-9,10-dihydroxy-(1α,4α,5α,8α)-1,4,5,8-tetrahydro-1,4:5,8-dimethanoanthracene

: 848486-27-1
1,4,5,8-tetrahydro-1,4:5,8-dimethanoanthracene-9,10-bis(phenylphosphonic acid ester)

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 1 h / 0 °C

2: 110 mg / aq. HCl / tetrahydrofuran; hexane

With hydrogenchloride; triethylamine; In tetrahydrofuran; hexane;
DOI:10.1002/chem.200400603