(CH₂)8(NCH₂COOH)3NCH₂CONCH(C₆H₅)2CH(C₁₀H₇)CONHCH₂C₆H₅

Base Information

• Chemical Name: (CH₂)8(NCH₂COOH)3NCH₂CONCH(C₆H₅)2CH(C₁₀H₇)CONHCH₂C₆H₅
• CAS No.: 1093225-18-3
• Molecular Formula: C₄₈H₅₄N₆O₈
• Molecular Weight: 842.992

Synonyms:(CH₂)8(NCH₂COOH)3NCH₂CONCH(C₆H₅)2CH(C₁₀H₇)CONHCH₂C₆H₅

Chemical Property of (CH₂)8(NCH₂COOH)3NCH₂CONCH(C₆H₅)2CH(C₁₀H₇)CONHCH₂C₆H₅

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Technology Process of (CH₂)8(NCH₂COOH)3NCH₂CONCH(C₆H₅)2CH(C₁₀H₇)CONHCH₂C₆H₅

There total 1 articles about (CH₂)8(NCH₂COOH)3NCH₂CONCH(C₆H₅)2CH(C₁₀H₇)CONHCH₂C₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-{[benzhydryl(benzylcarbamoylnaphthalen-1-ylmethyl)carbamoyl]methyl}-7,10-bis(ethoxycarbonylmethyl)-1,4,7,10-tetraazacyclododec-1-yl)acetic acid ethyl ester (1093225-14-9) → (CH2)8(NCH2COOH)3NCH2CONCH(C6H5)2CH(C10H7)CONHCH2C6H5 (1093225-18-3)

Guidance literature:

With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1039/b810083g

Reference yield: 99.0%

(CH2)8(NCH2COOH)3NCH2CONCH(C6H5)2CH(C10H7)CONHCH2C6H5 (1093225-18-3) + ytterbium(III) triflate (54761-04-5) → (CH2)8(NCH2COO)3NCH2CONCH(C6H5)2CHC10H7CONHCH2C6H5Yb (1093225-26-3)

Guidance literature:

In methanol; Yb triflate reacted with 1 equiv. of ligand in CH3OH at 40°C for 3 d;

DOI:10.1039/b810083g

Reference yield: 99.0%

(CH2)8(NCH2COOH)3NCH2CONCH(C6H5)2CH(C10H7)CONHCH2C6H5 (1093225-18-3) + europium(III) trifluoromethanesulfonate (52093-25-1) → (CH2)8(NCH2COO)3NCH2CONCH(C6H5)2CHC10H7CONHCH2C6H5Eu (1093225-24-1)

Guidance literature:

In methanol; Eu triflate reacted with 1 equiv. of ligand in CH3OH at 40°C for 3 d;

DOI:10.1039/b810083g

upstream raw materials:

(4-{[benzhydryl(benzylcarbamoylnaphthalen-1-ylmethyl)carbamoyl]methyl}-7,10-bis(ethoxycarbonylmethyl)-1,4,7,10-tetraazacyclododec-1-yl)acetic acid ethyl ester

Downstream raw materials:

(CH₂)8(NCH₂COO)3NCH₂CONCH(C₆H₅)2CHC₁₀H₇CONHCH₂C₆H₅Yb

(CH₂)8(NCH₂COO)3NCH₂CONCH(C₆H₅)2CHC₁₀H₇CONHCH₂C₆H₅Eu

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