Technology Process of C16H24ClNOS
There total 3 articles about C16H24ClNOS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C10H19NOS; (4-chlorphenyl)magnesium bromide;
In
dichloromethane;
at -50 - 20 ℃;
Inert atmosphere;
With
water; ammonium chloride;
In
dichloromethane;
Inert atmosphere;
DOI:10.1021/ol3000519
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1-methyl-1H-imidazole; [2,2]bipyridinyl; tetrakis(actonitrile)copper(I) hexafluorophosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen / acetonitrile / 20 °C
2.1: titanium(IV) tetraethanolate / tetrahydrofuran / 20 °C / Inert atmosphere
3.1: dichloromethane / -50 - 20 °C / Inert atmosphere
3.2: Inert atmosphere
With
1-methyl-1H-imidazole; [2,2]bipyridinyl; titanium(IV) tetraethanolate; tetrakis(actonitrile)copper(I) hexafluorophosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ol3000519
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 20 °C / Inert atmosphere
2.1: dichloromethane / -50 - 20 °C / Inert atmosphere
2.2: Inert atmosphere
With
titanium(IV) tetraethanolate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ol3000519
