IrCl(P(CH₃)3)3(C₈H₁₂)

Base Information

Chemical Name:IrCl(P(CH₃)3)3(C₈H₁₂)
CAS No.:118494-48-7
Molecular Formula:C₁₇H₃₉IrP₃*Cl
Molecular Weight:564.091
Hs Code.:

IrCl(P(CH<sub>3</sub>)3)3(C<sub>8</sub>H<sub>12</sub>)

Synonyms:IrCl(P(CH₃)3)3(C₈H₁₂)

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Chemical Property of IrCl(P(CH₃)3)3(C₈H₁₂)

Chemical Property:

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Technology Process of IrCl(P(CH₃)3)3(C₈H₁₂)

There total 1 articles about IrCl(P(CH₃)3)3(C₈H₁₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102525-11-1
(η⁵-indenyl)(η⁴-1,5-cyclooctadiene)iridium(I)

: 594-09-2
trimethylphosphane

: 118494-48-7
[tris-(trimethylphosphine)(cyclooctadiene)iridium(I)]chloride

: 18053-75-3
3-Trimethylsilylinden

Guidance literature:: With (CH₃)3SiCl; In tetrahydrofuran; addn.;

Reference yield: 91.0%

: 118494-48-7
[tris-(trimethylphosphine)(cyclooctadiene)iridium(I)]chloride

: 6921-34-2
benzylmagnesium chloride

: (2-benzylcyclooct-5-en-1-yl)tris(trimethylphosphine)iridium(I)

Guidance literature:: In tetrahydrofuran; reaction under N2: addn. of soln. of benzylmagnesium chloride in THF to a slurry of Ir-compd. in the same solvent, stirring at room temp. overnight; removal of solvent under vac., extn. with pentane, slow evapn. of pentane with cooling, elem. anal.;
DOI:10.1016/0020-1693(94)03903-8

Reference yield: 85.0%

: 118494-48-7
[tris-(trimethylphosphine)(cyclooctadiene)iridium(I)]chloride

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 148424-90-2
mer-(Me₃P)3Ir(O₂CC₆H₄OH)(H)(Cl)

Guidance literature:: In tetrahydrofuran; byproducts: COD; (N2), heated and stirred at 60°C for 8 h; solvent removed under vacuum, washed with ether, reprecipitated from THF by addn. of pentane, collected, dried under vacuum, elem. anal.;