cyclo-ε-(benzyloxy)-L-α-amino-δ-adipamidyl)>

Base Information

Chemical Name:cyclo-ε-(benzyloxy)-L-α-amino-δ-adipamidyl)>
CAS No.:96195-04-9
Molecular Formula:C₄₅H₅₇N₉O₁₂
Molecular Weight:916.001
Hs Code.:

cyclo-<triglycyltris(N<sup>ε</sup>-(benzyloxy)-L-α-amino-δ-adipamidyl)>

Synonyms:cyclo-ε-(benzyloxy)-L-α-amino-δ-adipamidyl)>

Suppliers and Price of cyclo-ε-(benzyloxy)-L-α-amino-δ-adipamidyl)>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of cyclo-ε-(benzyloxy)-L-α-amino-δ-adipamidyl)>

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of cyclo-ε-(benzyloxy)-L-α-amino-δ-adipamidyl)>

There total 5 articles about cyclo-ε-(benzyloxy)-L-α-amino-δ-adipamidyl)> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 96195-01-6
H-Gly-3-(Gly)2-ONp TFA

: 96195-04-9
cyclo-ε-(benzyloxy)-L-α-amino-δ-adipamidyl)>

Guidance literature:: With 4-methyl-morpholine; pyridine; In N,N-dimethyl-formamide; at 60 - 65 ℃; for 10h;
DOI:10.1021/jo00213a013

Reference yield: 33.0%

: 96195-03-8
H-Gly-3-(Gly)2-OH TFA

: 96195-04-9
cyclo-ε-(benzyloxy)-L-α-amino-δ-adipamidyl)>

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; In dichloromethane; N,N-dimethyl-formamide; 1.) 0 deg C, 1 h, 2.) RT, 4 d;
DOI:10.1021/jo00213a013

Reference yield:

: 96195-29-8
Boc-Gly-3-(Gly)2-OH

: 96195-04-9
cyclo-ε-(benzyloxy)-L-α-amino-δ-adipamidyl)>

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / pyridine, 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride / dimethylformamide / 36 h / Ambient temperature

2: 87 percent / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 54 percent / N-methylmorpholine, pyridine / dimethylformamide / 10 h / 60 - 65 °C

With 4-methyl-morpholine; pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00213a013