3-(2-oxo-oxazolidine-3-carbonyl)-6-trityloxy-hexanoic acid trityloxy-amide

Base Information

Chemical Name:3-(2-oxo-oxazolidine-3-carbonyl)-6-trityloxy-hexanoic acid trityloxy-amide
CAS No.:928618-03-5
Molecular Formula:C₄₈H₄₄N₂O₆
Molecular Weight:744.887
Hs Code.:

Synonyms:3-(2-oxo-oxazolidine-3-carbonyl)-6-trityloxy-hexanoic acid trityloxy-amide

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Chemical Property of 3-(2-oxo-oxazolidine-3-carbonyl)-6-trityloxy-hexanoic acid trityloxy-amide

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Technology Process of 3-(2-oxo-oxazolidine-3-carbonyl)-6-trityloxy-hexanoic acid trityloxy-amide

There total 8 articles about 3-(2-oxo-oxazolidine-3-carbonyl)-6-trityloxy-hexanoic acid trityloxy-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 913987-03-8
6-hydroxy-3-(2-oxooxazolidine-3-carbonyl)-N-(trityloxy)hexanamide

: 76-83-5
trityl chloride

: 928618-03-5
3-(2-oxo-oxazolidine-3-carbonyl)-6-trityloxy-hexanoic acid trityloxy-amide

Guidance literature:: With dmap; TEA; In dichloromethane; at 20 ℃;
DOI:10.1039/b609446e

Reference yield:

: 913987-01-6
3-(5-(benzyloxy)pentanoyl)oxazolidin-2-one

: 928618-03-5
3-(2-oxo-oxazolidine-3-carbonyl)-6-trityloxy-hexanoic acid trityloxy-amide

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / NaHMDS

2: 99 percent / TFA / CH₂Cl₂

3: 80 percent / DCC / CH₂Cl₂

4: 75 percent / H₂ / Pd/C / tetrahydrofuran / 1.5 h / 20 °C

5: 98 percent / DMAP; TEA / CH₂Cl₂ / 20 °C

With dmap; TEA; hydrogen; sodium hexamethyldisilazane; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b609446e

Reference yield:

: 913987-02-7
6-(benzyloxy)-3-(2-oxooxazolidine-3-carbonyl)hexanoic acid

: 928618-03-5
3-(2-oxo-oxazolidine-3-carbonyl)-6-trityloxy-hexanoic acid trityloxy-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / DCC / CH₂Cl₂

2: 75 percent / H₂ / Pd/C / tetrahydrofuran / 1.5 h / 20 °C

3: 98 percent / DMAP; TEA / CH₂Cl₂ / 20 °C

With dmap; TEA; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b609446e