bis-1,5-[methyl-6-azido-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-(3-oxapentane)

Base Information

Chemical Name:bis-1,5-[methyl-6-azido-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-(3-oxapentane)
CAS No.:1283056-63-2
Molecular Formula:C₄₆H₅₆N₆O₁₁
Molecular Weight:868.984
Hs Code.:

Synonyms:bis-1,5-[methyl-6-azido-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-(3-oxapentane)

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Chemical Property of bis-1,5-[methyl-6-azido-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-(3-oxapentane)

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Technology Process of bis-1,5-[methyl-6-azido-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-(3-oxapentane)

There total 1 articles about bis-1,5-[methyl-6-azido-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-(3-oxapentane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 7460-82-4
diethylene glycol ditosylate

: 54522-58-6
methyl 6-azido-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranoside

: 1283056-63-2
bis-1,5-[methyl-6-azido-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-(3-oxapentane)

Guidance literature:: With tetrabutylammomium bromide; sodium hydroxide; In water; toluene; at 40 ℃; for 72h;
DOI:10.1016/j.crci.2010.03.032

Reference yield: 94.0%

: 1283056-63-2
bis-1,5-[methyl-6-azido-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-(3-oxapentane)

: 1283056-65-4
bis-1,5-[methyl-6-amino-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-(3-oxapentane)

Guidance literature:: With 5%-palladium/activated carbon; triethylamine; In methanol; for 24h;
DOI:10.1016/j.crci.2010.03.032

Reference yield:

: 1283056-63-2
bis-1,5-[methyl-6-azido-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-(3-oxapentane)

: 1283056-68-7
bis-1,5-[methyl-2,3-di-O-benzyl-6-deoxy-6-tosylamino-4-yloxy-α-D-glucopyranoside]-(3-oxapentane)

Guidance literature:: Multi-step reaction with 2 steps

1: 5%-palladium/activated carbon; triethylamine / methanol / 24 h

2: pyridine / 48 h / -20 °C

With pyridine; 5%-palladium/activated carbon; triethylamine; In methanol;
DOI:10.1016/j.crci.2010.03.032