Technology Process of Carbamodithioic acid, bis(2,2,2-trifluoroethyl)-, lithium salt
There total 1 articles about Carbamodithioic acid, bis(2,2,2-trifluoroethyl)-, lithium salt which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
bis(2,2,2-trifluoroethyl)amine;
With
n-butyllithium;
In
diethyl ether;
for 1h;
cooling;
carbon disulfide;
In
diethyl ether;
at 0 - 20 ℃;
DOI:10.1021/je0502952
- Guidance literature:
-
With
PEt2Ph; toluene;
In
tetrahydrofuran;
treatment of MoO2Cl2 and PEt2Ph in THF (5 min), addn. of Li-compnd. in THF, filtration after 2 h; solvent removal, washing (EtOH), drying (vacuum), recrystn. (toluene); elem. anal.;