trans-6,13-bis(phenylthio)-6,13-dihydropentacene

Base Information

Chemical Name:trans-6,13-bis(phenylthio)-6,13-dihydropentacene
CAS No.:894773-47-8
Molecular Formula:C₃₄H₂₄S₂
Molecular Weight:496.697
Hs Code.:

Synonyms:trans-6,13-bis(phenylthio)-6,13-dihydropentacene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-6,13-bis(phenylthio)-6,13-dihydropentacene

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Technology Process of trans-6,13-bis(phenylthio)-6,13-dihydropentacene

There total 2 articles about trans-6,13-bis(phenylthio)-6,13-dihydropentacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 108-98-5
thiophenol

: 783321-44-8
trans-6,13-dihydroxy-6,13-dihydropentacene

: 894773-47-8
trans-6,13-bis(phenylthio)-6,13-dihydropentacene

Guidance literature:: With zinc(II) iodide; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/ol060679x

Reference yield:

: 3029-32-1
6,13-pentacenequinone

: 894773-47-8
trans-6,13-bis(phenylthio)-6,13-dihydropentacene

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / NaBH₄ / methanol / 1.5 h / 0 - 20 °C

2: 73 percent / zinc iodide / CH₂Cl₂ / 2 h / 20 °C

With sodium tetrahydroborate; zinc(II) iodide; In methanol; dichloromethane;
DOI:10.1021/ol060679x