Technology Process of C13H19NO
There total 14 articles about C13H19NO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C13H15NO;
With
borane-THF;
In
tetrahydrofuran;
at 20 ℃;
for 18h;
With
water; sodium hydrogencarbonate;
In
tetrahydrofuran;
- Guidance literature:
-
With
ethanolamine;
In
toluene;
at 70 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: copper(I) bromide; lithium bromide / tetrahydrofuran / 18 h / 0 °C / Inert atmosphere
2.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 1 h / 50 °C
2.2: pH 1
3.1: potassium hydroxide; water; sodium tetrahydroborate / 2 h / 10 - 20 °C
4.1: trifluoroacetic acid / dichloromethane / 18 h / 20 °C
5.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C
5.2: -78 - 20 °C
6.1: dmap; triethylamine / dichloromethane / 1 h / 0 - 20 °C
7.1: boron trifluoride diethyl etherate / acetonitrile / 18 h / 20 °C / Inert atmosphere
8.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C
9.1: DAICEL AS-H / hexane; ethanol / Resolution of racemate
10.1: borane-THF / tetrahydrofuran / 18 h / 20 °C
With
dmap; sodium tetrahydroborate; borane-THF; lithium hydroxide monohydrate; boron trifluoride diethyl etherate; potassium tert-butylate; water; diisobutylaluminium hydride; triethylamine; trifluoroacetic acid; potassium hydroxide; copper(I) bromide; lithium bromide;
In
tetrahydrofuran; ethanol; hexane; dichloromethane; acetonitrile;
