C₃₇H₅₆O₆Si₂

Base Information

Chemical Name:C₃₇H₅₆O₆Si₂
CAS No.:1350544-17-0
Molecular Formula:C₃₇H₅₆O₆Si₂
Molecular Weight:653.019
Hs Code.:

C<sub>37</sub>H<sub>56</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₃₇H₅₆O₆Si₂

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Chemical Property of C₃₇H₅₆O₆Si₂

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Technology Process of C₃₇H₅₆O₆Si₂

There total 8 articles about C₃₇H₅₆O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1350544-16-9
C₃₇H₅₆O₅Si₂

: 1350544-17-0
C₃₇H₅₆O₆Si₂

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - -5 ℃; for 7h; Inert atmosphere;
DOI:10.1021/ol202728v

Reference yield:

: 1350544-09-0
C₂₄H₃₆O₅Si

: 1350544-17-0
C₃₇H₅₆O₆Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: titanium tetrachloride / toluene / 1.17 h / -78 °C / Inert atmosphere

1.2: 3.5 h / -78 - 5 °C

2.1: 1,1,1,3,3,3-hexamethyl-disilazane; sodium iodide / acetonitrile / 3 h / 82 °C / Inert atmosphere

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 3 h / 23 °C / Inert atmosphere

4.1: diethylzinc / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

4.2: 0.67 h / -78 - 0 °C / Inert atmosphere

4.3: 0.42 h / -78 - -20 °C / Inert atmosphere

5.1: cerium(III) chloride; lithium chloride / diethyl ether / 3.25 h / -78 °C / Inert atmosphere

5.2: 2 h / -78 - 0 °C / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / benzene / 4.5 h / 23 °C / Inert atmosphere

7.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 7 h / -78 - -5 °C / Inert atmosphere

With cerium(III) chloride; diethylzinc; pyridinium p-toluenesulfonate; titanium tetrachloride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; 1,1,1,3,3,3-hexamethyl-disilazane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; lithium chloride; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; acetonitrile; benzene; 1.1: Diels-Alder reaction / 1.2: Diels-Alder reaction;
DOI:10.1021/ol202728v

Reference yield:

: C₂₄H₃₈O₅Si

: 1350544-17-0
C₃₇H₅₆O₆Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 0 °C / Inert atmosphere

2.1: titanium tetrachloride / toluene / 1.17 h / -78 °C / Inert atmosphere

2.2: 3.5 h / -78 - 5 °C

3.1: 1,1,1,3,3,3-hexamethyl-disilazane; sodium iodide / acetonitrile / 3 h / 82 °C / Inert atmosphere

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 3 h / 23 °C / Inert atmosphere

5.1: diethylzinc / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

5.2: 0.67 h / -78 - 0 °C / Inert atmosphere

5.3: 0.42 h / -78 - -20 °C / Inert atmosphere

6.1: cerium(III) chloride; lithium chloride / diethyl ether / 3.25 h / -78 °C / Inert atmosphere

6.2: 2 h / -78 - 0 °C / Inert atmosphere

7.1: pyridinium p-toluenesulfonate / benzene / 4.5 h / 23 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 7 h / -78 - -5 °C / Inert atmosphere

With cerium(III) chloride; diethylzinc; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; titanium tetrachloride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; 1,1,1,3,3,3-hexamethyl-disilazane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; lithium chloride; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene; acetonitrile; benzene; 1.1: Parikh-Doering oxidation / 2.1: Diels-Alder reaction / 2.2: Diels-Alder reaction;
DOI:10.1021/ol202728v