tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)

Base Information

• Chemical Name: tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)
• CAS No.: 97878-01-8
• Molecular Formula: C₈H₂₀N*C₂₄H₈F₁₇O₂Si
• Molecular Weight: 809.638

Synonyms:tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)

Chemical Property of tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)

There total 6 articles about tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(TB-5-11)-bis-(1,1,1,3,3,3-hexafluoro-2-phenyl-propan-2-olato(2-)-C2',O)-phenyl-silicate(1-); lithium salt (70083-67-9) → tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>(pentafluorophenyl)silicate(1-) (97878-01-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 59.6 percent / CH₂Cl₂

2: 72 percent / Br₂ / 24 h / 25 °C

3: Li / 1.) THF; 2.) ether, -78 deg C, then 25 deg C, 1 h

With bromine; lithium; In dichloromethane;

DOI:10.1021/ja00308a030

Reference yield:

Tetramethylammonium Bis<α,α-bis(trifluoromethyl)-benzenemethanolato(2-)-C2,O>phenylsilicate (70083-69-1) → tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>(pentafluorophenyl)silicate(1-) (97878-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / Br₂ / 24 h / 25 °C

2: Li / 1.) THF; 2.) ether, -78 deg C, then 25 deg C, 1 h

With bromine; lithium;

DOI:10.1021/ja00308a030

Reference yield:

tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>phenylsilicate(1-) (97878-00-7) → tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>(pentafluorophenyl)silicate(1-) (97878-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / Br₂ / 24 h / 25 °C

2: Li / 1.) THF; 2.) ether, -78 deg C, then 25 deg C, 1 h

With bromine; lithium;

DOI:10.1021/ja00308a030

upstream raw materials:

Pentafluorobenzene

tetraethylammonium bromide

C₁₈H₈F₁₂O₂Si

(TB-5-11)-bis-(1,1,1,3,3,3-hexafluoro-2-phenyl-propan-2-olato^(2-)-C^2',O)-phenyl-silicate^(1-); lithium salt

Downstream raw materials:

lithium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>-phenoxysilicate (1-)

tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato (2-)-C²,O>(4-methoxyphenyl)silicate(1-)

tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato (2-)-C²,O><3-(trifluoromethyl)phenyl>silicate(1-)

tetrabutylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 97878-01-8 tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>(pentafluorophenyl)silicate(1-)

Send

Send

Metric Ton KG G Pound L ML

Send

Send