N-(5-Brom-4-benzoxycarbonylamino-2-methyl-3-thienyl)-N-cyanglycinmethylester

Base Information

Chemical Name:N-(5-Brom-4-benzoxycarbonylamino-2-methyl-3-thienyl)-N-cyanglycinmethylester
CAS No.:78648-52-9
Molecular Formula:C₁₈H₁₈BrN₃O₄S
Molecular Weight:452.329
Hs Code.:

Synonyms:N-(5-Brom-4-benzoxycarbonylamino-2-methyl-3-thienyl)-N-cyanglycinmethylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(5-Brom-4-benzoxycarbonylamino-2-methyl-3-thienyl)-N-cyanglycinmethylester

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Technology Process of N-(5-Brom-4-benzoxycarbonylamino-2-methyl-3-thienyl)-N-cyanglycinmethylester

There total 2 articles about N-(5-Brom-4-benzoxycarbonylamino-2-methyl-3-thienyl)-N-cyanglycinmethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 506-68-3
bromocyane

: 78648-50-7
N-(4-Benzoxycarbonylamino-5-brom-2-methyl-3-thienyl)-glycinmethylester

: 78648-52-9
N-(5-Brom-4-benzoxycarbonylamino-2-methyl-3-thienyl)-N-cyanglycinmethylester

Guidance literature:: With sodium carbonate; In methanol; for 0.25h; Ambient temperature;
DOI:10.1002/ardp.19813140613

Reference yield:

: 78648-48-3
N-(2-Brom-4-brommethyl-5-methyl-3-thienyl)-carbaminsaeurebenzylester

: 78648-52-9
N-(5-Brom-4-benzoxycarbonylamino-2-methyl-3-thienyl)-N-cyanglycinmethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / NaH / methanol / 0.67 h / Heating

2: 97 percent / Na₂CO₃ / methanol / 0.25 h / Ambient temperature

With sodium hydride; sodium carbonate; In methanol;
DOI:10.1002/ardp.19813140613