2-azi-4-oxobutyl-2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Base Information

• Chemical Name: 2-azi-4-oxobutyl-2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside
• CAS No.: 160540-02-3
• Molecular Formula: C₃₈H₄₀N₂O₇
• Molecular Weight: 636.745
• Mol file: 160540-02-3.mol

Synonyms:2-azi-4-oxobutyl-2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Chemical Property of 2-azi-4-oxobutyl-2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-azi-4-oxobutyl-2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

There total 1 articles about 2-azi-4-oxobutyl-2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2-azi-4-hydroxybutyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (141242-44-6) → 2-azi-4-oxobutyl-2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (160540-02-3)

Guidance literature:

With dipyridinium dichromate; In benzene; for 18h;

DOI:10.1016/0008-6215(94)00225-8

Reference yield: 67.0%

2-azi-4-oxobutyl-2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (160540-02-3) → 2-azi-4-hydroxy-4-<3H>butyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (160540-03-4)

Guidance literature:

With sodium boron [ 3H]hydride; water; In 1,4-dioxane;

DOI:10.1016/0008-6215(94)00225-8

Reference yield:

2-azi-4-oxobutyl-2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (160540-02-3) → C45H39(3)HN2O13S

Guidance literature:

Multi-step reaction with 3 steps

1: 67 percent / NaB⁽³⁾H₄, water / dioxane

2: 80 percent / pyridine / CH₂Cl₂ / 84 h / Ambient temperature

3: NaOAc, O₃ / CH₂Cl₂ / 1 h / 0 °C

With pyridine; sodium boron [ 3H]hydride; water; sodium acetate; ozone; In 1,4-dioxane; dichloromethane;

DOI:10.1016/0008-6215(94)00225-8

upstream raw materials:

2-azi-4-hydroxybutyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Downstream raw materials:

2-azi-4-hydroxy-4-<3H>butyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside