6-amino-N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

Base Information

Chemical Name:6-amino-N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine
CAS No.:852057-88-6
Molecular Formula:C₅₀H₇₅N₅O₈S₄
Molecular Weight:1002.44
Hs Code.:

6-amino-N<sup>1</sup>,N<sup>12</sup>-diethyl-N<sup>1</sup>,N<sup>4</sup>,N<sup>9</sup>,N<sup>12</sup>-tetrakis(mesitylenesulfonyl)spermine

Synonyms:6-amino-N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

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Chemical Property of 6-amino-N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

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Technology Process of 6-amino-N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

There total 4 articles about 6-amino-N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 852057-87-5
N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

: 852057-88-6
6-amino-N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

Guidance literature:: N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine; With sodium tetrahydroborate; In dichloromethane; water; isopropyl alcohol; at 20 ℃; for 18h;

With acetic acid; In dichloromethane; isopropyl alcohol; at 80 ℃; for 18h;
DOI:10.1021/jm050024m

Reference yield:

: 852057-85-3
N¹,N¹²-diethyl-6-hydroxy-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

: 852057-88-6
6-amino-N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 61 percent / pyridine / CH₂Cl₂ / 24 h / 20 °C

2.1: 62 percent / dimethylformamide / 18 h / 85 °C

3.1: NaBH₄ / CH₂Cl₂; H₂O; propan-2-ol / 18 h / 20 °C

3.2: 74 percent / aq. acetic acid / CH₂Cl₂; propan-2-ol / 18 h / 80 °C

With pyridine; sodium tetrahydroborate; In dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm050024m

Reference yield:

: 852057-86-4
N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)-6-(p-toluenesulfonato)spermine

: 852057-88-6
6-amino-N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 62 percent / dimethylformamide / 18 h / 85 °C

2.1: NaBH₄ / CH₂Cl₂; H₂O; propan-2-ol / 18 h / 20 °C

2.2: 74 percent / aq. acetic acid / CH₂Cl₂; propan-2-ol / 18 h / 80 °C

With sodium tetrahydroborate; In dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm050024m