2-benzoxazolyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:2-benzoxazolyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside
CAS No.:1095998-68-7
Molecular Formula:C₅₇H₄₉NO₁₆S
Molecular Weight:1036.08
Hs Code.:

Synonyms:2-benzoxazolyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

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Chemical Property of 2-benzoxazolyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

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Technology Process of 2-benzoxazolyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

There total 1 articles about 2-benzoxazolyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 133411-30-0
ethyl [2,6-di-O-benzoyl-3,4-O-(1-methylethylidene)-β-D-galactopyranosyl]-(1->4)-2,3,6-tri-O-benzoyl-1-thio-β-D-glucopyranoside

: potassium salt of 2-mercaptobenzoxazole

: 1095998-68-7
2-benzoxazolyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

Guidance literature:: ethyl [2,6-di-O-benzoyl-3,4-O-(1-methylethylidene)-β-D-galactopyranosyl]-(1->4)-2,3,6-tri-O-benzoyl-1-thio-β-D-glucopyranoside; With bromine; In dichloromethane; at 20 ℃; for 0.0833333h; Molecular sieve; Inert atmosphere;

potassium salt of 2-mercaptobenzoxazole; In acetone; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/b810569c

Reference yield:

: 1095998-50-7
4-(pyridin-2-yl)thiazole-2-yl 3-O-acetyl-6-O-(tert-butyl)diphenylsilyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 1095998-68-7
2-benzoxazolyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

: 744245-95-2
2-thiazolinyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-galactopyranoside

: 4-(pyridin-2-yl)thiazole-2-yl O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->6)-3-O-acetyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: 4-(pyridin-2-yl)thiazole-2-yl 3-O-acetyl-6-O-(tert-butyl)diphenylsilyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside; With palladium(II) bromide; In 1,2-dichloro-ethane; at 20 ℃; Inert atmosphere; Molecular sieve;

2-thiazolinyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-galactopyranoside; With silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; Inert atmosphere; Molecular sieve;

2-benzoxazolyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside; Further stages;
DOI:10.1039/b810569c