bis(trifluorothioacetyl) disulfide

Base Information

• Chemical Name: bis(trifluorothioacetyl) disulfide
• CAS No.: 21690-87-9
• Molecular Formula: C₄F₆O₂S₂
• Molecular Weight: 258.165

Synonyms:bis(trifluorothioacetyl) disulfide

Chemical Property of bis(trifluorothioacetyl) disulfide

Chemical Property:

Purity/Quality:

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Technology Process of bis(trifluorothioacetyl) disulfide

There total 2 articles about bis(trifluorothioacetyl) disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

bis(fluorosulfuryl) peroxide (13709-32-5) + trifluorothioacetic acid (2925-25-9) → trifluoroacetyl fluosulfate (5762-53-8) + bis(trifluorothioacetyl) disulfide (21690-87-9) + fluorosulphonic acid (7789-21-1)

Guidance literature:

equimolar mixt. of educts;

DOI:10.1021/ic50130a028

Reference yield:

bis(fluorosulfuryl) peroxide (13709-32-5) + trifluorothioacetic acid (2925-25-9) → bis(trifluorothioacetyl) disulfide (21690-87-9)

Guidance literature:

warming CF3C(O)SH - S2O6F2 mixt. (1:0.5) from -183 to +25°C;

DOI:10.1021/ic50130a028

Reference yield:

bis(trifluorothioacetyl) disulfide (21690-87-9) → hydrogen sulfide (7783-06-4) + sulfur (7704-34-9) + trifluoroacetic acid (76-05-1)

Guidance literature:

With H₂O;

DOI:10.1021/jo01264a097

upstream raw materials:

bis(fluorosulfuryl) peroxide

trifluorothioacetic acid

Downstream raw materials:

hydrogen sulfide

sulfur

trifluoroacetic acid

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