Technology Process of C15H15FO5
There total 11 articles about C15H15FO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Candida antarctica-derived lipase A (NOVOZYM CALAL) immobilized on Toyonite 200M;
In
acetone;
at 25 ℃;
for 21h;
Enzymatic reaction;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylaluminum / hexane; tetrahydrofuran / 0.5 h / -60 - -50 °C
1.2: 2.75 h / -50 - -40 °C
1.3: 0.5 h / 5 °C
2.1: Candida antarctica-derived lipase A (NOVOZYM CALAL) immobilized on Toyonite 200M / acetone / 21 h / 25 °C / Enzymatic reaction
With
triethylaluminum;
Candida antarctica-derived lipase A (NOVOZYM CALAL) immobilized on Toyonite 200M;
In
tetrahydrofuran; hexane; acetone;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium chloride / water; dimethyl sulfoxide / 2 h / 130 °C
2.1: tert.-butylhydroperoxide / bis(acetylacetonate)oxovanadium / toluene; chlorobenzene / 4.17 h / 20 - 60 °C
3.1: triethylaluminum / hexane; tetrahydrofuran / 0.5 h / -60 - -50 °C
3.2: 2.75 h / -50 - -40 °C
3.3: 0.5 h / 5 °C
4.1: Candida antarctica-derived lipase A (NOVOZYM CALAL) immobilized on Toyonite 200M / acetone / 21 h / 25 °C / Enzymatic reaction
With
tert.-butylhydroperoxide; triethylaluminum; lithium chloride;
bis(acetylacetonate)oxovanadium;
In
tetrahydrofuran; hexane; water; dimethyl sulfoxide; chlorobenzene; acetone; toluene;