methyl 2-O-acetyl-6-O-[2-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranosyl]-3-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

Base Information

• Chemical Name: methyl 2-O-acetyl-6-O-[2-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranosyl]-3-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside
• CAS No.: 1061302-65-5
• Molecular Formula: C₄₃H₆₂Br₂O₁₅Si₂
• Molecular Weight: 1034.94

Synonyms:methyl 2-O-acetyl-6-O-[2-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranosyl]-3-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

Chemical Property of methyl 2-O-acetyl-6-O-[2-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranosyl]-3-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

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Technology Process of methyl 2-O-acetyl-6-O-[2-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranosyl]-3-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

There total 1 articles about methyl 2-O-acetyl-6-O-[2-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranosyl]-3-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

methyl 2-O-acetyl-6-O-[2-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranosyl]-3-O-(tert-butyldimethylsilyl)-4-O-(4-methoxybenzyl)-α-D-glucopyranoside (1061302-51-9) → methyl 2-O-acetyl-6-O-[2-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranosyl]-3-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside (1061302-65-5)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 20 ℃;

DOI:10.1021/jo801184q

Reference yield: 63.0%

methyl 2-O-acetyl-6-O-[2-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranosyl]-3-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside (1061302-65-5) → methyl 6-O-[4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-α-D-glucopyranoside (1061302-74-6)

Guidance literature:

With methanol; acetyl chloride; In diethyl ether;

DOI:10.1021/jo801184q

upstream raw materials:

methyl 2-O-acetyl-6-O-[2-O-acetyl-4,6-bis-O-(4-bromobenzoyl)-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranosyl]-3-O-(tert-butyldimethylsilyl)-4-O-(4-methoxybenzyl)-α-D-glucopyranoside

Downstream raw materials:

methyl 6-O-[4,6-bis-O-(4-bromobenzoyl)-β-D-glucopyranosyl]-α-D-glucopyranoside

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