C₁₇H₂₂N₂O₅

Base Information

• Chemical Name: C₁₇H₂₂N₂O₅
• CAS No.: 1373521-77-7
• Molecular Formula: C₁₇H₂₂N₂O₅
• Molecular Weight: 334.372
• Mol file: 1373521-77-7.mol

Synonyms:C₁₇H₂₂N₂O₅

Chemical Property of C₁₇H₂₂N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₂N₂O₅

There total 4 articles about C₁₇H₂₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C17H24O5 (1373521-70-0) → C17H22N2O5 (1373521-77-7)

Guidance literature:

With 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 22h;

DOI:10.1016/j.tet.2012.03.009

Reference yield:

o-Hydroxyethylbenzene (90-00-6) → C17H22N2O5 (1373521-77-7)

Guidance literature:

Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 96 h / 20 °C

2: pyridine / dichloromethane / 0 - 20 °C

3: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 22 h / 20 °C

With pyridine; di-isopropyl azodicarboxylate; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile; 1: Mitsunobu reaction;

DOI:10.1016/j.tet.2012.03.009

Reference yield:

C13H20O2 (1373521-56-2) → C17H22N2O5 (1373521-77-7)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C

2: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 22 h / 20 °C

With pyridine; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; acetonitrile;

DOI:10.1016/j.tet.2012.03.009

upstream raw materials:

o-Hydroxyethylbenzene

C₁₇H₂₄O₅

C₁₃H₂₀O₂

(2R,4R)-pentanediol