{triruthenium(μ3-η2-diphenylacetylene)(μ-η2-bis(diphenylphosphino)methane)heptacarbonyl}

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Chemical Name:{triruthenium(μ3-η2-diphenylacetylene)(μ-η2-bis(diphenylphosphino)methane)heptacarbonyl}
CAS No.:136629-66-8
Molecular Formula:C₄₆H₃₂O₇P₂Ru₃
Molecular Weight:1061.91
Hs Code.:

Synonyms:{triruthenium(μ3-η2-diphenylacetylene)(μ-η2-bis(diphenylphosphino)methane)heptacarbonyl}

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Chemical Property of {triruthenium(μ3-η2-diphenylacetylene)(μ-η2-bis(diphenylphosphino)methane)heptacarbonyl}

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Technology Process of {triruthenium(μ3-η2-diphenylacetylene)(μ-η2-bis(diphenylphosphino)methane)heptacarbonyl}

There total 3 articles about {triruthenium(μ3-η2-diphenylacetylene)(μ-η2-bis(diphenylphosphino)methane)heptacarbonyl} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: {triruthenium(μ3-η2-diphenylacetylene)(μ-η2-bis(diphenylphosphino)methane)(μ-carbonyl)(heptacarbonyl)}

: 136629-66-8
{triruthenium(μ3-η2-diphenylacetylene)(μ-η2-bis(diphenylphosphino)methane)heptacarbonyl}

Guidance literature:: In tetrahydrofuran; byproducts: CO; refluxing for 1 h under inert gas; chromatographic purification (CH2Cl2/hexane), crystn. from the same solvent mixture, elem. anal.;

Reference yield: 79.0%

: Ru3(μ-PhCCPh)(CO)7(bis(diphenylphosphino)methane)

: 136629-66-8
{triruthenium(μ3-η2-diphenylacetylene)(μ-η2-bis(diphenylphosphino)methane)heptacarbonyl}

Guidance literature:: In benzene; N2-atmosphere; refluxing (70 - 80°C, 1 h); evapn. (reduced pressure), chromy. (CH2Cl2 / hexane = 1 : 4); elem. anal.;
DOI:10.1021/om950835w

Reference yield:

: {bis(triphenylphosphine)nitrogen}{triruthenium(μ-Cl)(μ3-η2-diphenylacetylene)(nonacarbonyl)}

: 2071-20-7
bis-diphenylphosphinomethane

: {triruthenium(μ3-η2-diphenylacetylene)(μ-η2-bis(diphenylphosphino)methane)(μ-carbonyl)(heptacarbonyl)}

: 136629-66-8
{triruthenium(μ3-η2-diphenylacetylene)(μ-η2-bis(diphenylphosphino)methane)heptacarbonyl}

: 21050-13-5
bis(triphenylphosphine)iminium chloride

Guidance literature:: In tetrahydrofuran; stoichiometric reaction between Ru-salt and 1 equiv of bis(diphenylphosphino)methane in THF during 30 min;