Technology Process of C17H21N2O4S(1-)*K(1+)
There total 6 articles about C17H21N2O4S(1-)*K(1+) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: mercury(II) diacetate / acetic acid / 0.5 h / 80 °C
1.2: 2 h / 80 - 85 °C
2.1: ozone / dichloromethane; methanol / 2 h / -78 °C
2.2: 20 °C
3.1: water; tetrahydrofuran / 4 h / 0 - 20 °C
4.1: potassium carbonate / N,N-dimethyl-formamide / 10 h / 60 °C
5.1: potassium hydroxide; water / methanol / 0.5 h / 20 °C
With
mercury(II) diacetate; water; potassium carbonate; ozone; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.5012/bkcs.2013.34.1.121
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ozone / dichloromethane; methanol / 2 h / -78 °C
1.2: 20 °C
2.1: water; tetrahydrofuran / 4 h / 0 - 20 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 10 h / 60 °C
4.1: potassium hydroxide; water / methanol / 0.5 h / 20 °C
With
water; potassium carbonate; ozone; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.5012/bkcs.2013.34.1.121