C₃₀H₃₂N₂O₂S

Base Information

Chemical Name:C₃₀H₃₂N₂O₂S
CAS No.:1355611-47-0
Molecular Formula:C₃₀H₃₂N₂O₂S
Molecular Weight:484.662
Hs Code.:

C<sub>30</sub>H<sub>32</sub>N<sub>2</sub>O<sub>2</sub>S

Synonyms:C₃₀H₃₂N₂O₂S

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Chemical Property of C₃₀H₃₂N₂O₂S

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Technology Process of C₃₀H₃₂N₂O₂S

There total 4 articles about C₃₀H₃₂N₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 4784-77-4,29576-14-5,39616-19-8
(E/Z)-crotyl bromide

: 1355611-22-1
C₂₆H₂₆N₂O₂S

: 1355611-47-0
C₃₀H₃₂N₂O₂S

Guidance literature:: (E/Z)-crotyl bromide; C₂₆H₂₆N₂O₂S; With ferric(III) bromide; In acetonitrile; at 45 - 50 ℃; Inert atmosphere;

With triethylamine; In tetrahydrofuran; acetonitrile; at -78 - 45 ℃; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/jo201753q

Reference yield:

: 1355611-19-6
C₂₆H₂₆N₂O₃

: 1355611-47-0
C₃₀H₃₂N₂O₂S

Guidance literature:: Multi-step reaction with 2 steps

1.1: Lawessons reagent; sodium hydrogencarbonate / toluene / 3 h / 120 °C

2.1: ferric(III) bromide / acetonitrile / 45 - 50 °C / Inert atmosphere

2.2: -78 - 45 °C

With Lawessons reagent; ferric(III) bromide; sodium hydrogencarbonate; In toluene; acetonitrile; 2.2: thio-Claisen rearrangement;
DOI:10.1021/jo201753q

Reference yield:

: 295328-85-7
(2S,5S)‐diphenylpyrrolidine

: 1355611-47-0
C₃₀H₃₂N₂O₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; triethylamine; dicyclohexyl-carbodiimide

2.1: Lawessons reagent; sodium hydrogencarbonate / toluene / 3 h / 120 °C

3.1: ferric(III) bromide / acetonitrile / 45 - 50 °C / Inert atmosphere

3.2: -78 - 45 °C

With Lawessons reagent; dmap; ferric(III) bromide; sodium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; In toluene; acetonitrile; 3.2: thio-Claisen rearrangement;
DOI:10.1021/jo201753q