2(R)-[(N-benzyloxy-N-formylamino)-methyl]-hexanoic acid pentafluorophenyl ester

Base Information

• Chemical Name: 2(R)-[(N-benzyloxy-N-formylamino)-methyl]-hexanoic acid pentafluorophenyl ester
• CAS No.: 301684-72-0
• Molecular Formula: C₂₁H₂₀F₅NO₄
• Molecular Weight: 445.386

Synonyms:2(R)-[(N-benzyloxy-N-formylamino)-methyl]-hexanoic acid pentafluorophenyl ester

Chemical Property of 2(R)-[(N-benzyloxy-N-formylamino)-methyl]-hexanoic acid pentafluorophenyl ester

Chemical Property:

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Technology Process of 2(R)-[(N-benzyloxy-N-formylamino)-methyl]-hexanoic acid pentafluorophenyl ester

There total 1 articles about 2(R)-[(N-benzyloxy-N-formylamino)-methyl]-hexanoic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

2,3,4,5,6-pentafluorophenol (771-61-9) + (2R)-2-({formyl[(phenylmethyl)oxy]amino}methyl)hexanoic acid (301685-23-4) → 2(R)-[(N-benzyloxy-N-formylamino)-methyl]-hexanoic acid pentafluorophenyl ester (301684-72-0)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 20 ℃;

Reference yield:

2(R)-[(N-benzyloxy-N-formylamino)-methyl]-hexanoic acid pentafluorophenyl ester (301684-72-0) + 2S-amino-1-[4-(4-methoxy-benzoyl)-piperidin-1-yl]-3,3-dimethyl-butan-1-one (325795-36-6) → 2R-[(benzyloxy-formyl-amino)-methyl]-hexanoic acid {1S-[4-(4-methoxy-benzoyl)-piperidine-1-carbonyl]-2,2-dimethyl-propyl}-amide (325795-35-5)

Guidance literature:

In dichloromethane; at 27 ℃;

Reference yield:

2(R)-[(N-benzyloxy-N-formylamino)-methyl]-hexanoic acid pentafluorophenyl ester (301684-72-0) + N-(2-pyridinyl)piperazine (20980-22-7) → C23H31N5O3 (1427032-50-5)

Guidance literature:

In dichloromethane; at 20 ℃; for 60h; Zymate XPH laboratory robot;

upstream raw materials:

2,3,4,5,6-pentafluorophenol

(2R)-2-({formyl[(phenylmethyl)oxy]amino}methyl)hexanoic acid

Downstream raw materials:

2R-[(benzyloxy-formyl-amino)-methyl]-hexanoic acid {1S-[4-(4-methoxy-benzoyl)-piperidine-1-carbonyl]-2,2-dimethyl-propyl}-amide

C₂₃H₃₁N₅O₃

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