N-<(3,6-dihydro-4-phenyl-1(2H)-pyridinyl)methylene>-1,1-dimethylethanamine

Base Information

Chemical Name:N-<(3,6-dihydro-4-phenyl-1(2H)-pyridinyl)methylene>-1,1-dimethylethanamine
CAS No.:123333-02-8
Molecular Formula:C₁₆H₂₂N₂
Molecular Weight:242.364
Hs Code.:

Synonyms:N-<(3,6-dihydro-4-phenyl-1(2H)-pyridinyl)methylene>-1,1-dimethylethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(3,6-dihydro-4-phenyl-1(2H)-pyridinyl)methylene>-1,1-dimethylethanamine

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Technology Process of N-<(3,6-dihydro-4-phenyl-1(2H)-pyridinyl)methylene>-1,1-dimethylethanamine

There total 1 articles about N-<(3,6-dihydro-4-phenyl-1(2H)-pyridinyl)methylene>-1,1-dimethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 10338-69-9
1,2,3,6-tetrahydro-4-phenylpyridine

: 23314-06-9
N,N-dimethyl-N'-tert-butylformamidine

: 123333-02-8
N-<(3,6-dihydro-4-phenyl-1(2H)-pyridinyl)methylene>-1,1-dimethylethanamine

Guidance literature:: With ammonium sulfate; In toluene; for 24h; Heating;
DOI:10.1021/jo00284a048

Reference yield:

: 123333-02-8
N-<(3,6-dihydro-4-phenyl-1(2H)-pyridinyl)methylene>-1,1-dimethylethanamine

: 1-Formyl-4-phenyl-1,2,5,6-tetrahydro-pyridine-2-carboxylic acid (2,6-dimethyl-phenyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 1 h, 2.) THF, hexane, a) -78 deg C, 30 min, b) RT, 3 h

2: 8 percent / H₂ / 10percent Pd/C / ethanol / 4 h / 2327.2 Torr

With n-butyllithium; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo00284a048

Reference yield:

: 123333-02-8
N-<(3,6-dihydro-4-phenyl-1(2H)-pyridinyl)methylene>-1,1-dimethylethanamine

: 1-Formyl-4-phenyl-1,2,5,6-tetrahydro-pyridine-2-carboxylic acid (4-ethoxy-2,6-dimethyl-phenyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 1 h, 2.) THF, hexane, a) -78 deg C, 30 min, b) RT, 3 h

2: 14 percent / H₂ / 10percent Pd/C / ethanol / 4 h / 2327.2 Torr

With n-butyllithium; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo00284a048