5-(N-(2-morpholinoethyl)methylsulfonamido)-2-(trifluoromethyl)benzoic acid

Base Information

Chemical Name:5-(N-(2-morpholinoethyl)methylsulfonamido)-2-(trifluoromethyl)benzoic acid
CAS No.:1610862-26-4
Molecular Formula:C₁₅H₁₉F₃N₂O₅S
Molecular Weight:396.387
Hs Code.:

Synonyms:5-(N-(2-morpholinoethyl)methylsulfonamido)-2-(trifluoromethyl)benzoic acid

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Chemical Property of 5-(N-(2-morpholinoethyl)methylsulfonamido)-2-(trifluoromethyl)benzoic acid

Chemical Property:

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Technology Process of 5-(N-(2-morpholinoethyl)methylsulfonamido)-2-(trifluoromethyl)benzoic acid

There total 6 articles about 5-(N-(2-morpholinoethyl)methylsulfonamido)-2-(trifluoromethyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1610862-27-5
benzyl 5-(N-(2-morpholinoethyl)methylsulfonamido)-2-(trifluoromethyl)benzoate

: 1610862-26-4
5-(N-(2-morpholinoethyl)methylsulfonamido)-2-(trifluoromethyl)benzoic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; ethyl acetate; for 6h; under 1551.49 Torr;

Reference yield:

: 1960-52-7
2-methyl-4-nitro-1-(trifluoromethyl)benzene

: 1610862-26-4
5-(N-(2-morpholinoethyl)methylsulfonamido)-2-(trifluoromethyl)benzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: periodic acid; chromium(VI) oxide / acetonitrile / 20 °C

2: caesium carbonate / acetonitrile / 0.5 h / 100 °C / Microwave irradiation

3: ammonium chloride; iron / water; ethanol / 1 h / 80 °C

4: pyridine / 0 - 20 °C

5: potassium carbonate / N,N-dimethyl-formamide / 3 h / 100 °C

6: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 6 h / 1551.49 Torr

With pyridine; chromium(VI) oxide; palladium 10% on activated carbon; hydrogen; iron; potassium carbonate; ammonium chloride; caesium carbonate; periodic acid; In methanol; ethanol; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1610862-29-7
benzyl 5-amino-2-(trifluoromethyl)benzoate

: 1610862-26-4
5-(N-(2-morpholinoethyl)methylsulfonamido)-2-(trifluoromethyl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 3 h / 100 °C

3: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 6 h / 1551.49 Torr

With pyridine; palladium 10% on activated carbon; hydrogen; potassium carbonate; In methanol; ethyl acetate; N,N-dimethyl-formamide;