C₁₇H₂₄O₅

Base Information

Chemical Name:C₁₇H₂₄O₅
CAS No.:1360148-07-7
Molecular Formula:C₁₇H₂₄O₅
Molecular Weight:308.375
Hs Code.:

C<sub>17</sub>H<sub>24</sub>O<sub>5</sub>

Synonyms:C₁₇H₂₄O₅

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Chemical Property of C₁₇H₂₄O₅

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Technology Process of C₁₇H₂₄O₅

There total 1 articles about C₁₇H₂₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 2746-25-0
p-Methoxybenzyl bromide

: (2R,3S,5S)-5,6-Epoxy-1,2-O-isopropylidenehexane-1,2,3-triol

: 1360148-07-7
C₁₇H₂₄O₅

Guidance literature:: (2R,3S,5S)-5,6-Epoxy-1,2-O-isopropylidenehexane-1,2,3-triol; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;

p-Methoxybenzyl bromide; In N,N-dimethyl-formamide; at 0 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.12.102

Reference yield: 96.0%

: 1360148-07-7
C₁₇H₂₄O₅

: 1360148-09-9
C₁₇H₂₆O₅

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/j.tetlet.2011.12.102

Reference yield:

: 1360148-07-7
C₁₇H₂₄O₅

: C₂₇H₃₆O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C

3.1: trifluoroacetic acid / dichloromethane; water / 20 °C

4.1: sodium periodate / tetrahydrofuran; water / 0.25 h / 20 °C

5.1: N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

5.2: -78 - 20 °C / Inert atmosphere

6.1: camphor-10-sulfonic acid / methanol / 2 h / 20 °C

With 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium periodate; lithium aluminium tetrahydride; camphor-10-sulfonic acid; sodium hexamethyldisilazane; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; 5.2: Julia-Lythgoe olefination;
DOI:10.1016/j.tetlet.2011.12.102