1-{2-[bis(pentafluorophenyl)boryl]benzyl}-2,2,6,6-tetramethylpiperidine

Base Information

• Chemical Name: 1-{2-[bis(pentafluorophenyl)boryl]benzyl}-2,2,6,6-tetramethylpiperidine
• CAS No.: 1072095-95-4
• Molecular Formula: C₂₈H₂₄BF₁₀N
• Molecular Weight: 575.3

Synonyms:1-{2-[bis(pentafluorophenyl)boryl]benzyl}-2,2,6,6-tetramethylpiperidine

Chemical Property of 1-{2-[bis(pentafluorophenyl)boryl]benzyl}-2,2,6,6-tetramethylpiperidine

Chemical Property:

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Technology Process of 1-{2-[bis(pentafluorophenyl)boryl]benzyl}-2,2,6,6-tetramethylpiperidine

There total 4 articles about 1-{2-[bis(pentafluorophenyl)boryl]benzyl}-2,2,6,6-tetramethylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

hydrido[bis(pentafluorophenyl)]{2-[(2,2,6,6-tetramethylpiperidinium-1-yl)methyl]phenyl}borate (1072095-96-5) → 1-{2-[bis(pentafluorophenyl)boryl]benzyl}-2,2,6,6-tetramethylpiperidine (1072095-95-4)

Guidance literature:

In toluene; a toluene-soln. was refluxed at 110°C in a closed system under reduced pressure or a flow of argon for 20 h;

DOI:10.1021/ja806627s

Reference yield: 70.0%

1-bromo-2-(2,2,6,6-tetramethylpiperidinylmethyl)benzene (891-48-5) + bis(pentafluorophenyl)boron chloride (2720-03-8) → 1-{2-[bis(pentafluorophenyl)boryl]benzyl}-2,2,6,6-tetramethylpiperidine (1072095-95-4)

Guidance literature:

1-bromo-2-(2,2,6,6-tetramethylpiperidinylmethyl)benzene; With tert.-butyl lithium; In diethyl ether; pentane; at -70 - 20 ℃; Inert atmosphere;

bis(pentafluorophenyl)boron chloride; In hexane; toluene; at -20 - 20 ℃;

DOI:10.1021/ja806627s

Reference yield:

C5H6(CH3)4N(2)HCH2C6H4B(C6F5)2(2)H → 1-{2-[bis(pentafluorophenyl)boryl]benzyl}-2,2,6,6-tetramethylpiperidine (1072095-95-4) + deuterium (16873-17-9,12184-84-8)

Guidance literature:

In toluene; 110°C, toluene;

DOI:10.1021/ja206394w

upstream raw materials:

1-bromo-2-(2,2,6,6-tetramethylpiperidinylmethyl)benzene

bis(pentafluorophenyl)boron chloride

hydrido[bis(pentafluorophenyl)]{2-[(2,2,6,6-tetramethylpiperidinium-1-yl)methyl]phenyl}borate

C₅H₆(CH₃)4N⁽²⁾HCH₂C₆H₄B(C₆F₅)2H

Downstream raw materials:

hydrido[bis(pentafluorophenyl)]{2-[(2,2,6,6-tetramethylpiperidinium-1-yl)methyl]phenyl}borate

C₅H₆(CH₃)4N⁽²⁾HCH₂C₆H₄B(C₆F₅)2H

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