C₂₆H₄₀N₅O₁₀PSi

Base Information

• Chemical Name: C₂₆H₄₀N₅O₁₀PSi
• CAS No.: 943301-10-8
• Molecular Formula: C₂₆H₄₀N₅O₁₀PSi
• Molecular Weight: 641.69
• Mol file: 943301-10-8.mol

Synonyms:C₂₆H₄₀N₅O₁₀PSi

Chemical Property of C₂₆H₄₀N₅O₁₀PSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₄₀N₅O₁₀PSi

There total 4 articles about C₂₆H₄₀N₅O₁₀PSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H33N5O8Si → C26H40N5O10PSi (943301-10-8)

Guidance literature:

Multi-step reaction with 4 steps

1: tetrahydrofuran / 1 h / 20 °C

2: 400 mg / t-BuOOH / tetrahydrofuran; decane / 1 h / 0 °C

3: H₂; iPr₂NEt / Pd/C / tetrahydrofuran / 2 h / 4137.29 Torr

4: pyridine / 1 h / 0 °C

With pyridine; tert.-butylhydroperoxide; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; decane;

DOI:10.1021/ja072174n

Reference yield:

C25H38N5O10SiP → C26H40N5O10PSi (943301-10-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 400 mg / t-BuOOH / tetrahydrofuran; decane / 1 h / 0 °C

2: H₂; iPr₂NEt / Pd/C / tetrahydrofuran / 2 h / 4137.29 Torr

3: pyridine / 1 h / 0 °C

With pyridine; tert.-butylhydroperoxide; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; decane;

DOI:10.1021/ja072174n

Reference yield:

C25H38N5O11SiP → C26H40N5O10PSi (943301-10-8)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂; iPr₂NEt / Pd/C / tetrahydrofuran / 2 h / 4137.29 Torr

2: pyridine / 1 h / 0 °C

With pyridine; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran;

DOI:10.1021/ja072174n

upstream raw materials:

formyl acetic anhydride

Downstream raw materials:

C₂₀H₂₆N₅O₁₀P