1-oxaspiro[2.5]octane-2-carboxylic acid

Base Information

Chemical Name:1-oxaspiro[2.5]octane-2-carboxylic acid
CAS No.:25957-47-5
Molecular Formula:C8H12 O3 . Na
Molecular Weight:178.163
Hs Code.:
Mol file:25957-47-5.mol

Synonyms:1-Oxaspiro[2.5]octane-2-carboxylicacid, sodium salt (6CI,7CI,8CI,9CI); NSC 147645

Suppliers and Price of 1-oxaspiro[2.5]octane-2-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 1-oxaspiro[2.5]octane-2-carboxylic acid

Chemical Property:

Vapor Pressure:0.000116mmHg at 25°C
Boiling Point:312.4°Cat760mmHg
Flash Point:131.4°C
Density:1.24g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-oxaspiro[2.5]octane-2-carboxylic acid

There total 2 articles about 1-oxaspiro[2.5]octane-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 33717-87-2,169611-36-3
1-oxa-spiro-[2,5]octane-2-carboxylic acid methyl ester

: 25957-47-5
Sodium; 1-oxa-spiro[2.5]octane-2-carboxylate

Guidance literature:: With sodium methylate; In methanol; added water, stand overnight;
DOI:10.1002/jhet.5570220512

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 25957-47-5
Sodium; 1-oxa-spiro[2.5]octane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium t-butoxide / 2-methyl-propan-2-ol / 12 h / 10 - 15 °C

2: 94 percent / sodium methoxide / methanol / added water, stand overnight

With potassium tert-butylate; sodium methylate; In methanol; tert-butyl alcohol;
DOI:10.1002/jhet.5570220512