2-Amino-N-{[(2-benzoyl-4-nitro-phenyl)-methyl-carbamoyl]-methyl}-acetamide

Base Information

Chemical Name:2-Amino-N-{[(2-benzoyl-4-nitro-phenyl)-methyl-carbamoyl]-methyl}-acetamide
CAS No.:76337-93-4
Molecular Formula:C₁₈H₁₈N₄O₅
Molecular Weight:370.365
Hs Code.:

Synonyms:2-Amino-N-{[(2-benzoyl-4-nitro-phenyl)-methyl-carbamoyl]-methyl}-acetamide

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Chemical Property of 2-Amino-N-{[(2-benzoyl-4-nitro-phenyl)-methyl-carbamoyl]-methyl}-acetamide

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Technology Process of 2-Amino-N-{[(2-benzoyl-4-nitro-phenyl)-methyl-carbamoyl]-methyl}-acetamide

There total 3 articles about 2-Amino-N-{[(2-benzoyl-4-nitro-phenyl)-methyl-carbamoyl]-methyl}-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.8%

: [({[(2-Benzoyl-4-nitro-phenyl)-methyl-carbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester

: 76337-93-4
2-Amino-N-{[(2-benzoyl-4-nitro-phenyl)-methyl-carbamoyl]-methyl}-acetamide

Guidance literature:: With hydrogen bromide; In acetic acid; for 2h; Ambient temperature;
DOI:10.1021/jm00133a006

Reference yield:

: 38249-89-7
[(2-Benzoyl-4-nitro-phenylcarbamoyl)-methyl]-carbamic acid benzyl ester

: 76337-93-4
2-Amino-N-{[(2-benzoyl-4-nitro-phenyl)-methyl-carbamoyl]-methyl}-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, oil, 2-5 deg C, 15 min, 2.) DMF, oil, 2-5 deg C, 2 h

2: 20percent HBr / acetic acid / 1 h / Ambient temperature

3: hexamethylphosphoric acid triamide; acetonitrile / 5 h / Ambient temperature

4: 80.8 percent / 30percent HBr / acetic acid / 2 h / Ambient temperature

With hydrogen bromide; sodium hydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; acetic acid; acetonitrile;
DOI:10.1021/jm00133a006

Reference yield:

: 64563-68-4
{[(2-Benzoyl-4-nitro-phenyl)-methyl-carbamoyl]-methyl}-carbamic acid benzyl ester

: 76337-93-4
2-Amino-N-{[(2-benzoyl-4-nitro-phenyl)-methyl-carbamoyl]-methyl}-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 20percent HBr / acetic acid / 1 h / Ambient temperature

2: hexamethylphosphoric acid triamide; acetonitrile / 5 h / Ambient temperature

3: 80.8 percent / 30percent HBr / acetic acid / 2 h / Ambient temperature

With hydrogen bromide; In N,N,N,N,N,N-hexamethylphosphoric triamide; acetic acid; acetonitrile;
DOI:10.1021/jm00133a006