Technology Process of C29H36O3
There total 4 articles about C29H36O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
formic acid; triethylamine;
palladium diacetate; triphenylphosphine;
In
1,4-dioxane;
for 72h;
Heating;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 60 percent / LDA / tetrahydrofuran / 1.) -78 deg C to -40 deg C, 2.) -78 deg C
2: 65 percent / HCO2H, NEt3 / PPh3/Pd(OAc)2 / dioxane / 72 h / Heating
With
formic acid; triethylamine; lithium diisopropyl amide;
palladium diacetate; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 88 percent / K2CO3, 18-crown-6 / 168 h / Ambient temperature
2: 60 percent / LDA / tetrahydrofuran / 1.) -78 deg C to -40 deg C, 2.) -78 deg C
3: 65 percent / HCO2H, NEt3 / PPh3/Pd(OAc)2 / dioxane / 72 h / Heating
With
formic acid; 18-crown-6 ether; potassium carbonate; triethylamine; lithium diisopropyl amide;
palladium diacetate; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane;