C₅₄H₇₄O₁₃SSi

Base Information Edit

Chemical Name:C₅₄H₇₄O₁₃SSi
CAS No.:1415891-64-3
Molecular Formula:C₅₄H₇₄O₁₃SSi
Molecular Weight:991.325
Hs Code.:
Mol file:1415891-64-3.mol

C<sub>54</sub>H<sub>74</sub>O<sub>13</sub>SSi

Synonyms:C₅₄H₇₄O₁₃SSi

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Chemical Property of C₅₄H₇₄O₁₃SSi Edit

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Technology Process of C₅₄H₇₄O₁₃SSi

There total 8 articles about C₅₄H₇₄O₁₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1415891-40-5
C₆₀H₈₈O₁₃SSi₂

: 1415891-64-3
C₅₄H₇₄O₁₃SSi

Guidance literature:: With toluene-4-sulfonic acid; In methanol; dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo302267f

Reference yield:

: 1415891-30-3
(2S,4aS,6R,7S,8aR)-7-(benzyloxy)-6-((benzyloxy)methyl)-2-(((2R,3S)-3-((tert-butyldimethylsilyl)oxy)tetrahydro-2H-pyran-2-yl)methyl)hexahydropyrano[3,2-b]pyran-3(2H)-one

: 1415891-64-3
C₅₄H₇₄O₁₃SSi

Guidance literature:: Multi-step reaction with 7 steps

1: toluene-4-sulfonic acid / chloroform / 7 h / 55 °C / Inert atmosphere

2: trimethylsilyl trifluoromethanesulfonate; triethylsilane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3: hydrogen; 10 wt% Pd(OH)2 on carbon / ethyl acetate / 18 h / 20 °C

4: 2,6-dimethylpyridine / tetrahydrofuran / 0.5 h / -80 °C / Inert atmosphere

5: tetrahydrofuran / 0.67 h / -80 °C / Inert atmosphere

6: n-butyllithium; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran; hexane / -100 °C / Inert atmosphere

7: toluene-4-sulfonic acid / dichloromethane; methanol / 1 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; triethylsilane; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; trimethylsilyl trifluoromethanesulfonate; 10 wt% Pd(OH)2 on carbon; hydrogen; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; chloroform; ethyl acetate;
DOI:10.1021/jo302267f

Reference yield:

: 1415891-57-4
(2R,3S,4aR,5aS,6aR,10aS,11aR,13aS)-3-(benzyloxy)-2-((benzyloxy)methyl)-11a-methoxytetradecahydro-2H-pyrano[3,2-b]pyrano[2',3':5,6]pyrano[2,3-f]oxepine

: 1415891-64-3
C₅₄H₇₄O₁₃SSi

Guidance literature:: Multi-step reaction with 6 steps

1: trimethylsilyl trifluoromethanesulfonate; triethylsilane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2: hydrogen; 10 wt% Pd(OH)2 on carbon / ethyl acetate / 18 h / 20 °C

3: 2,6-dimethylpyridine / tetrahydrofuran / 0.5 h / -80 °C / Inert atmosphere

4: tetrahydrofuran / 0.67 h / -80 °C / Inert atmosphere

5: n-butyllithium; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran; hexane / -100 °C / Inert atmosphere

6: toluene-4-sulfonic acid / dichloromethane; methanol / 1 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; triethylsilane; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; trimethylsilyl trifluoromethanesulfonate; 10 wt% Pd(OH)2 on carbon; hydrogen; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; ethyl acetate;
DOI:10.1021/jo302267f