N-[(2'-benzyloxy)-3'-methoxy-6'-bromobenzyl]-6,7-(methylenedioxy)-1-naphthylamine

Base Information

Chemical Name:N-[(2'-benzyloxy)-3'-methoxy-6'-bromobenzyl]-6,7-(methylenedioxy)-1-naphthylamine
CAS No.:142886-76-8
Molecular Formula:C₂₆H₂₂BrNO₄
Molecular Weight:492.369
Hs Code.:

Synonyms:N-[(2'-benzyloxy)-3'-methoxy-6'-bromobenzyl]-6,7-(methylenedioxy)-1-naphthylamine

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Chemical Property of N-[(2'-benzyloxy)-3'-methoxy-6'-bromobenzyl]-6,7-(methylenedioxy)-1-naphthylamine

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Technology Process of N-[(2'-benzyloxy)-3'-methoxy-6'-bromobenzyl]-6,7-(methylenedioxy)-1-naphthylamine

There total 5 articles about N-[(2'-benzyloxy)-3'-methoxy-6'-bromobenzyl]-6,7-(methylenedioxy)-1-naphthylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [1-(2-Benzyloxy-6-bromo-3-methoxy-phenyl)-meth-(Z)-ylidene]-naphtho[2,3-d][1,3]dioxol-5-yl-amine

: 142886-76-8
N-[(2'-benzyloxy)-3'-methoxy-6'-bromobenzyl]-6,7-(methylenedioxy)-1-naphthylamine

Guidance literature:: With dimethylamine borane; acetic acid; In toluene; for 1h; Ambient temperature;
DOI:10.1021/jo9718758

Reference yield:

: 20035-41-0
6-bromo-2-hydroxy-3-methoxybenzaldehyde

: 142886-76-8
N-[(2'-benzyloxy)-3'-methoxy-6'-bromobenzyl]-6,7-(methylenedioxy)-1-naphthylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / K₂CO₃, KI / methanol / 9 h / Heating

2: toluene / 1.5 h / Heating

3: 664 g / dimethylamineborane, acetic acid / toluene / 1 h / Ambient temperature

With dimethylamine borane; potassium carbonate; acetic acid; potassium iodide; In methanol; toluene;
DOI:10.1021/jo9718758

Reference yield:

: 100-44-7
benzyl chloride

: 142886-76-8
N-[(2'-benzyloxy)-3'-methoxy-6'-bromobenzyl]-6,7-(methylenedioxy)-1-naphthylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / K₂CO₃, KI / methanol / 9 h / Heating

2: toluene / 1.5 h / Heating

3: 664 g / dimethylamineborane, acetic acid / toluene / 1 h / Ambient temperature

With dimethylamine borane; potassium carbonate; acetic acid; potassium iodide; In methanol; toluene;
DOI:10.1021/jo9718758