(2S,6R)-6-Amino-2-benzyloxycarbonylamino-6-hydrazinocarbonyl-hexanoic acid

Base Information

Chemical Name:(2S,6R)-6-Amino-2-benzyloxycarbonylamino-6-hydrazinocarbonyl-hexanoic acid
CAS No.:79338-38-8
Molecular Formula:C₁₅H₂₂N₄O₅
Molecular Weight:338.363
Hs Code.:

Synonyms:(2S,6R)-6-Amino-2-benzyloxycarbonylamino-6-hydrazinocarbonyl-hexanoic acid

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Chemical Property of (2S,6R)-6-Amino-2-benzyloxycarbonylamino-6-hydrazinocarbonyl-hexanoic acid

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Technology Process of (2S,6R)-6-Amino-2-benzyloxycarbonylamino-6-hydrazinocarbonyl-hexanoic acid

There total 1 articles about (2S,6R)-6-Amino-2-benzyloxycarbonylamino-6-hydrazinocarbonyl-hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76489-90-2
(2S,6R)-2-Benzyloxycarbonylamino-6-tert-butoxycarbonylamino-7-(N'-tert-butoxycarbonyl-hydrazino)-7-oxo-heptanoic acid

: 79338-38-8
(2S,6R)-6-Amino-2-benzyloxycarbonylamino-6-hydrazinocarbonyl-hexanoic acid

Guidance literature:: With trifluoroacetic acid; Ambient temperature;
DOI:10.1021/jm00346a001

Reference yield:

: 79338-38-8
(2S,6R)-6-Amino-2-benzyloxycarbonylamino-6-hydrazinocarbonyl-hexanoic acid

: 79337-68-1
(2S,6R)-2-Amino-6-benzyloxycarbonylamino-heptanedioic acid

Guidance literature:: With sodium periodate; sulfuric acid; In water; at 0 ℃; Yield given;
DOI:10.1021/jm00346a001

Reference yield:

: 79338-38-8
(2S,6R)-6-Amino-2-benzyloxycarbonylamino-6-hydrazinocarbonyl-hexanoic acid

: 79334-23-9
N-stearoyl-γ-D-Glu(α-OBzl)-(L)-Boc-(D)meso-A₂pm

Guidance literature:: Multi-step reaction with 4 steps

1: NaIO₄, 0.1 N H₂SO₄ / H₂O / 0 °C

2: 100 percent / Et₃N / acetone; H₂O

3: 81 percent / H₂ / 10percent Pd/C / acetic acid

4: 1.) isobutyl chloroformate, N-methylmorpholine / 1.) CH₂Cl₂, from -15 to -10 deg C, 2.) from -10 to 0 deg C

With 4-methyl-morpholine; sodium periodate; sulfuric acid; hydrogen; triethylamine; isobutyl chloroformate; palladium on activated charcoal; In water; acetic acid; acetone;
DOI:10.1021/jm00346a001