N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin

Base Information

Chemical Name:N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin
CAS No.:107033-42-1
Molecular Formula:C₂₅H₃₄N₄O₉S
Molecular Weight:566.632
Hs Code.:

Synonyms:N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin

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Chemical Property of N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin

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Technology Process of N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin

There total 10 articles about N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 107033-41-0
N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin-γ-benzylester

: 107033-42-1
N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin

Guidance literature:: With sodium cyanide; In tetrahydrofuran; for 6h; Ambient temperature;

Reference yield:

: 106947-89-1
Methyl-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-β-D-glucofuranosid

: 107033-42-1
N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin

Guidance literature:: Multi-step reaction with 8 steps

1: 58 percent / DCC, DMAP / tetrahydrofuran / 24 h / Ambient temperature

2: 58 percent / pyridine / 16 h / -10 °C

3: 54 percent / pyridine / 16 h / Ambient temperature

4: 93 percent / CH₃ONa / tetrahydrofuran / 0.5 h / 0 °C

5: 45 percent / DCC / ethyl acetate / 1.) 0 deg C, 30 min, 2.) room temp., 5 h

6: 42 percent / (C₆H₅)3PS, CF₃COOH / CHCl₃ / 12 h / 40 °C

7: 62 percent / Et₃N / dimethylformamide / 1 h / Ambient temperature

8: 93 percent / 1.) aq. NaCN / tetrahydrofuran / 6 h / Ambient temperature

With pyridine; dmap; sodium cyanide; sodium methylate; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine sulfide; trifluoroacetic acid; In tetrahydrofuran; chloroform; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 106947-97-1
Methyl-2-benzamido-2-desoxy-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucofuranosid

: 107033-42-1
N-<2-O-(Methyl-2-benzamido-2,3,5,6-tetradesoxy-5,6-epithio-β-D-glucofuranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamin

Guidance literature:: Multi-step reaction with 7 steps

1: 58 percent / pyridine / 16 h / -10 °C

2: 54 percent / pyridine / 16 h / Ambient temperature

3: 93 percent / CH₃ONa / tetrahydrofuran / 0.5 h / 0 °C

4: 45 percent / DCC / ethyl acetate / 1.) 0 deg C, 30 min, 2.) room temp., 5 h

5: 42 percent / (C₆H₅)3PS, CF₃COOH / CHCl₃ / 12 h / 40 °C

6: 62 percent / Et₃N / dimethylformamide / 1 h / Ambient temperature

7: 93 percent / 1.) aq. NaCN / tetrahydrofuran / 6 h / Ambient temperature

With pyridine; sodium cyanide; sodium methylate; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine sulfide; trifluoroacetic acid; In tetrahydrofuran; chloroform; ethyl acetate; N,N-dimethyl-formamide;