(4S,5S)-4-Bromo-5-hydroxy-cyclohexane-1,2-dicarboxylic acid dimethyl ester

Base Information

Chemical Name:(4S,5S)-4-Bromo-5-hydroxy-cyclohexane-1,2-dicarboxylic acid dimethyl ester
CAS No.:77743-51-2
Molecular Formula:C₁₀H₁₅BrO₅
Molecular Weight:295.13
Hs Code.:

Synonyms:(4S,5S)-4-Bromo-5-hydroxy-cyclohexane-1,2-dicarboxylic acid dimethyl ester

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Chemical Property of (4S,5S)-4-Bromo-5-hydroxy-cyclohexane-1,2-dicarboxylic acid dimethyl ester

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Technology Process of (4S,5S)-4-Bromo-5-hydroxy-cyclohexane-1,2-dicarboxylic acid dimethyl ester

There total 4 articles about (4S,5S)-4-Bromo-5-hydroxy-cyclohexane-1,2-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 4841-84-3
dimethyl cis-1,2,3,6-tetrahydrophthalate

: 77743-51-2
(4S,5S)-4-Bromo-5-hydroxy-cyclohexane-1,2-dicarboxylic acid dimethyl ester

Guidance literature:: With sulfuric acid; hydrogen bromide; In water; acetonitrile; for 3.14h; electr. 3.3 mA/cm²;
DOI:10.1021/jo00329a032

Reference yield: 50.0%

: 4841-84-3
dimethyl cis-1,2,3,6-tetrahydrophthalate

: 26595-80-2,26595-97-1,77841-42-0,90409-98-6
(1S,2R)-4,5-Dibromo-cyclohexane-1,2-dicarboxylic acid dimethyl ester

: 77743-51-2
(1R,2S)-4-Bromo-5-hydroxy-cyclohexane-1,2-dicarboxylic acid dimethyl ester

Guidance literature:: With N-Bromosuccinimide; In water; at 25 ℃; Rate constant; Product distribution; micellar effect (cetyltrimethylammonium bromide), effect of NaBr;
DOI:10.1021/jo00009a019

Reference yield:

: 4841-84-3
dimethyl cis-1,2,3,6-tetrahydrophthalate

: 77743-51-2
(4S,5S)-4-Bromo-5-hydroxy-cyclohexane-1,2-dicarboxylic acid dimethyl ester

: 77841-42-0
(4S,5S)-4,5-Dibromo-cyclohexane-1,2-dicarboxylic acid dimethyl ester

Guidance literature:: With sulfuric acid; sodium bromide; In water; acetonitrile; 1.) Electrochem_. bromofunctionalization, 2.) Correlation between conc. Br^- and the distribution of the prod.;
DOI:10.1021/jo00329a032