13-hydroxy-9-(1-hydroxyethyl)-3-[5-methoxy-5-(2,4,6-tribromo-3-hydroxyphenyl)pentan-2-yl]-4,14,16,16-tetramethyl-2,6,10,17-tetraoxatricyclo[11.3.1.1~1,5~]octadecane-7,11-dione (non-preferred name)

Base Information

Chemical Name:13-hydroxy-9-(1-hydroxyethyl)-3-[5-methoxy-5-(2,4,6-tribromo-3-hydroxyphenyl)pentan-2-yl]-4,14,16,16-tetramethyl-2,6,10,17-tetraoxatricyclo[11.3.1.1~1,5~]octadecane-7,11-dione (non-preferred name)
CAS No.:90359-02-7
Molecular Formula:C₃₂H₄₅Br₃O₁₀
Molecular Weight:829.415
Hs Code.:

13-hydroxy-9-(1-hydroxyethyl)-3-[5-methoxy-5-(2,4,6-tribromo-3-hydroxyphenyl)pentan-2-yl]-4,14,16,16-tetramethyl-2,6,10,17-tetraoxatricyclo[11.3.1.1~1,5~]octadecane-7,11-dione (non-preferred name)

Synonyms:19,21-dibromoaplysiatoxin

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Chemical Property of 13-hydroxy-9-(1-hydroxyethyl)-3-[5-methoxy-5-(2,4,6-tribromo-3-hydroxyphenyl)pentan-2-yl]-4,14,16,16-tetramethyl-2,6,10,17-tetraoxatricyclo[11.3.1.1~1,5~]octadecane-7,11-dione (non-preferred name)

Chemical Property:

Vapor Pressure:6.94E-28mmHg at 25°C

Purity/Quality:

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Technology Process of 13-hydroxy-9-(1-hydroxyethyl)-3-[5-methoxy-5-(2,4,6-tribromo-3-hydroxyphenyl)pentan-2-yl]-4,14,16,16-tetramethyl-2,6,10,17-tetraoxatricyclo[11.3.1.1~1,5~]octadecane-7,11-dione (non-preferred name)

There total 2 articles about 13-hydroxy-9-(1-hydroxyethyl)-3-[5-methoxy-5-(2,4,6-tribromo-3-hydroxyphenyl)pentan-2-yl]-4,14,16,16-tetramethyl-2,6,10,17-tetraoxatricyclo[11.3.1.1~1,5~]octadecane-7,11-dione (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52423-28-6
debromo aplysiatoxin

: 90414-33-8
19-bromodebromoaplysiatoxin

: 52659-57-1
aplysiatoxin

: 66648-18-8
19-bromoaplysiatoxin

: 90359-02-7
19,21-dibromoaplysiatoxin

Guidance literature:: With bromine; sodium phosphate; sodium bromide; In methanol; Ambient temperature; 1) pH 6, 2) pH 8;
DOI:10.1021/jo00187a035