2-[2,3-dichloro-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Base Information

Chemical Name:2-[2,3-dichloro-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole
CAS No.:1370243-97-2
Molecular Formula:C₂₁H₁₆Cl₂N₂O₄S
Molecular Weight:463.341
Hs Code.:

Synonyms:2-[2,3-dichloro-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

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Chemical Property of 2-[2,3-dichloro-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

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Technology Process of 2-[2,3-dichloro-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

There total 7 articles about 2-[2,3-dichloro-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₃Cl₂N₃O₄S

: 1370243-97-2
2-[2,3-dichloro-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Guidance literature:: With sodium hydrogencarbonate; In water; at 85 ℃; for 0.666667h;
DOI:10.1016/j.bmc.2012.02.011

Reference yield:

: 1370244-62-4
2-(4-butyryl-2,3-dichlorophenoxy)acetamide

: 1370243-97-2
2-[2,3-dichloro-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Guidance literature:: Multi-step reaction with 4 steps

1: tetraphosphorus decasulfide / tetrahydrofuran / 1.5 h / 50 °C

2: methanol / 24 h / Reflux

3: acetic acid / 1.5 h / 100 °C

4: sodium hydrogencarbonate / water / 0.67 h / 85 °C

With tetraphosphorus decasulfide; sodium hydrogencarbonate; acetic acid; In tetrahydrofuran; methanol; water; 3: Mannich reaction;
DOI:10.1016/j.bmc.2012.02.011

Reference yield:

: 1370244-48-6
2-[2,3-dichloro-4-(1-oxo-butyl) phenoxy]ethanethioamide

: 1370243-97-2
2-[2,3-dichloro-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 24 h / Reflux

2: acetic acid / 1.5 h / 100 °C

3: sodium hydrogencarbonate / water / 0.67 h / 85 °C

With sodium hydrogencarbonate; acetic acid; In methanol; water; 2: Mannich reaction;
DOI:10.1016/j.bmc.2012.02.011