Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆

Base Information

• Chemical Name: Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆
• CAS No.: 87114-84-9
• Molecular Formula: C₄₈H₅₆ClFeN₆*F₆P
• Molecular Weight: 953.277

Synonyms:Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆

Chemical Property of Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆

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Technology Process of Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆

There total 1 articles about Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)6(NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

Fe(py)2Cl2 (15616-26-9) + H4(CH2)6(NCH2C6H5CC6H5C3HCH3N2(CH2)3)2(4+)*3PF6(1-)*Cl(1-)=(H4(CH2)6(NCH2C6H5CC6H5C3HCH3N2(CH2)3)2)(PF6)3Cl → Cl(CH2)6(NCH2C6H5CC6H5C3HCH3N2(CH2)3)2Fe(1+)*PF6(1-)=(Cl(CH2)6(NCH2C6H5CC6H5C3HCH3N2(CH2)3)2Fe)PF6 (87114-84-9)

Guidance literature:

With triethylamine; In acetonitrile; ligand and slight excess of Fe complex slurring in MeCN, large excess of Et3N adding, refluxing for 5 min, cooling and filtering through celite, solvent removing, residue dissolving in hot MeOH, stirring for 10 min,filtering; purified by recrystn. from MeCN/EtOH or MeOH, identified by elem. anal.;

DOI:10.1021/ja00360a008

upstream raw materials:

Fe(py)2Cl₂

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