(1R,2S,3R,4S)-N-<4-<4-(2-Methoxyphenyl)-1-piperazinyl>butyl>-2,3-bicyclo<2.2.1>heptanedicarboximide

Base Information

Chemical Name:(1R*,2S*,3R*,4S*)-N-<4-<4-(2-Methoxyphenyl)-1-piperazinyl>butyl>-2,3-bicyclo<2.2.1>heptanedicarboximide
CAS No.:116753-39-0
Molecular Formula:C₂₄H₃₃N₃O₃
Molecular Weight:411.544
Hs Code.:

Synonyms:(1R*,2S*,3R*,4S*)-N-<4-<4-(2-Methoxyphenyl)-1-piperazinyl>butyl>-2,3-bicyclo<2.2.1>heptanedicarboximide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R*,2S*,3R*,4S*)-N-<4-<4-(2-Methoxyphenyl)-1-piperazinyl>butyl>-2,3-bicyclo<2.2.1>heptanedicarboximide

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Technology Process of (1R*,2S*,3R*,4S*)-N-<4-<4-(2-Methoxyphenyl)-1-piperazinyl>butyl>-2,3-bicyclo<2.2.1>heptanedicarboximide

There total 5 articles about (1R*,2S*,3R*,4S*)-N-<4-<4-(2-Methoxyphenyl)-1-piperazinyl>butyl>-2,3-bicyclo<2.2.1>heptanedicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.5%

: 120664-98-4
(1S,2R,6S,7R)-4-{4-[4-(2-Methoxy-phenyl)-piperazin-1-yl]-but-2-ynyl}-4-aza-tricyclo[5.2.1.0^2,6]decane-3,5-dione

: 116753-39-0
(1R*,2S*,3R*,4S*)-N-<4-<4-(2-Methoxyphenyl)-1-piperazinyl>butyl>-2,3-bicyclo<2.2.1>heptanedicarboximide

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; Ambient temperature;
DOI:10.1248/cpb.39.2288

Reference yield:

: 105981-36-0
N-Propargylbicyclo<2.2.1>heptane-2,3-di-exo-carboximide

: 116753-39-0
(1R*,2S*,3R*,4S*)-N-<4-<4-(2-Methoxyphenyl)-1-piperazinyl>butyl>-2,3-bicyclo<2.2.1>heptanedicarboximide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / copper sulfate / dioxane; H₂O / 70 - 80 °C

2: 90.5 percent / H₂ / 10percent Pd/C / tetrahydrofuran / Ambient temperature

With copper(I) sulfate; hydrogen; copper(II) sulfate; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1248/cpb.39.2288

Reference yield:

: 14805-29-9,1318027-24-5
(3aR,4S,7R,7aS)?4,7?methylene?1H?isoindole?1,3(2H)-dione

: 116753-39-0
(1R*,2S*,3R*,4S*)-N-<4-<4-(2-Methoxyphenyl)-1-piperazinyl>butyl>-2,3-bicyclo<2.2.1>heptanedicarboximide

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / K₂CO₃ / acetone / 1 h / Heating

2: 100 percent / copper sulfate / dioxane; H₂O / 70 - 80 °C

3: 90.5 percent / H₂ / 10percent Pd/C / tetrahydrofuran / Ambient temperature

With copper(I) sulfate; hydrogen; potassium carbonate; copper(II) sulfate; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; water; acetone;
DOI:10.1248/cpb.39.2288