C₆₈H₈₁NO₁₆

Base Information

Chemical Name:C₆₈H₈₁NO₁₆
CAS No.:1374760-29-8
Molecular Formula:C₆₈H₈₁NO₁₆
Molecular Weight:1168.39
Hs Code.:

C<sub>68</sub>H<sub>81</sub>NO<sub>16</sub>

Synonyms:C₆₈H₈₁NO₁₆

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Chemical Property of C₆₈H₈₁NO₁₆

Chemical Property:

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Technology Process of C₆₈H₈₁NO₁₆

There total 21 articles about C₆₈H₈₁NO₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374760-28-7
C₇₀H₈₃NO₁₇

: 108-24-7
acetic anhydride

: 1374760-29-8
C₆₈H₈₁NO₁₆

Guidance literature:: With tri-n-butyl-tin hydride; Pd(Ph)4; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 1374760-26-5
C₄₇H₅₉NO₁₄

: 1374760-29-8
C₆₈H₈₁NO₁₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / acetonitrile / 1.33 h / 0 °C

2.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

2.2: 20 °C

3.1: tri-n-butyl-tin hydride / Pd(Ph)4 / dichloromethane / 1 h / 20 °C

With tri-n-butyl-tin hydride; di(n-butyl)tin oxide; triethylamine; Pd(Ph)4; In methanol; dichloromethane; acetonitrile;

Reference yield:

: C₁₆H₂₃NO₁₀

: 1374760-29-8
C₆₈H₈₁NO₁₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.5 h / 20 °C

2.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

2.2: 2 h / 0 °C

3.1: sodium methylate; methanol / 2 h

3.2: IR-120 (H⁽¹⁺⁾) resin

4.1: triethylamine / acetonitrile / 1.33 h / 0 °C

5.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

5.2: 20 °C

6.1: tri-n-butyl-tin hydride / Pd(Ph)4 / dichloromethane / 1 h / 20 °C

With methanol; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; Pd(Ph)4; In methanol; dichloromethane; acetonitrile;