7-(4-chlorophenyl)-4,5-dihydro-7H-pyrano<3,4-c>isoxazole-3-carboaldehyde

Base Information

Chemical Name:7-(4-chlorophenyl)-4,5-dihydro-7H-pyrano<3,4-c>isoxazole-3-carboaldehyde
CAS No.:226984-05-0
Molecular Formula:C₁₃H₁₀ClNO₃
Molecular Weight:263.68
Hs Code.:

Synonyms:7-(4-chlorophenyl)-4,5-dihydro-7H-pyrano<3,4-c>isoxazole-3-carboaldehyde

Suppliers and Price of 7-(4-chlorophenyl)-4,5-dihydro-7H-pyrano<3,4-c>isoxazole-3-carboaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-(4-chlorophenyl)-4,5-dihydro-7H-pyrano<3,4-c>isoxazole-3-carboaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-(4-chlorophenyl)-4,5-dihydro-7H-pyrano<3,4-c>isoxazole-3-carboaldehyde

There total 4 articles about 7-(4-chlorophenyl)-4,5-dihydro-7H-pyrano<3,4-c>isoxazole-3-carboaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 226984-02-7
7-(4-chlorophenyl)-3-hydroxymethyl-4,5-dihydro-7H-pyrano<3,4-c>isoxazole

: 226984-05-0
7-(4-chlorophenyl)-4,5-dihydro-7H-pyrano<3,4-c>isoxazole-3-carboaldehyde

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; Ambient temperature;
DOI:10.1271/bbb.63.494

Reference yield:

: 38996-32-6
5-(tetrahydropyran-2-yloxy)-3-pentyn-1-ol

: 226984-05-0
7-(4-chlorophenyl)-4,5-dihydro-7H-pyrano<3,4-c>isoxazole-3-carboaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / NaH

2: 76 percent / PhNCO, Et₃N / benzene

3: 93 percent / TsOH*H₂O / methanol / 25 °C

4: 89 percent / PCC / CH₂Cl₂ / Ambient temperature

With sodium hydride; phenyl isocyanate; toluene-4-sulfonic acid; triethylamine; pyridinium chlorochromate; In methanol; dichloromethane; benzene;
DOI:10.1271/bbb.63.494

Reference yield:

: 226983-99-9
7-(4-chlorophenyl)-3-(tetrahydropyran-2-yloxymethyl)-4,5-dihydro-7H-pyrano<3,4-c>isoxazole

: 226984-05-0
7-(4-chlorophenyl)-4,5-dihydro-7H-pyrano<3,4-c>isoxazole-3-carboaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / TsOH*H₂O / methanol / 25 °C

2: 89 percent / PCC / CH₂Cl₂ / Ambient temperature

With toluene-4-sulfonic acid; pyridinium chlorochromate; In methanol; dichloromethane;
DOI:10.1271/bbb.63.494