benzyl imino(4-{[({3-methoxy-4-[(2-phenylethyl)amino]-1,1'-biphenyl-2-yl}acetyl)amino]methyl}phenyl)methylcarbamate

Base Information

Chemical Name:benzyl imino(4-{[({3-methoxy-4-[(2-phenylethyl)amino]-1,1'-biphenyl-2-yl}acetyl)amino]methyl}phenyl)methylcarbamate
CAS No.:361337-06-6
Molecular Formula:C₃₉H₃₈N₄O₄
Molecular Weight:626.755
Hs Code.:

Synonyms:benzyl imino(4-{[({3-methoxy-4-[(2-phenylethyl)amino]-1,1'-biphenyl-2-yl}acetyl)amino]methyl}phenyl)methylcarbamate

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Chemical Property of benzyl imino(4-{[({3-methoxy-4-[(2-phenylethyl)amino]-1,1'-biphenyl-2-yl}acetyl)amino]methyl}phenyl)methylcarbamate

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Technology Process of benzyl imino(4-{[({3-methoxy-4-[(2-phenylethyl)amino]-1,1'-biphenyl-2-yl}acetyl)amino]methyl}phenyl)methylcarbamate

There total 6 articles about benzyl imino(4-{[({3-methoxy-4-[(2-phenylethyl)amino]-1,1'-biphenyl-2-yl}acetyl)amino]methyl}phenyl)methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 361337-00-0
methyl (6-hydroxy-2-methoxy-3-nitrophenyl)acetate

: 361337-06-6
benzyl imino(4-{[({3-methoxy-4-[(2-phenylethyl)amino]-1,1'-biphenyl-2-yl}acetyl)amino]methyl}phenyl)methylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: 83 percent / Et₃N / CH₂Cl₂ / 20 °C

2.1: 74 percent / (Ph₃P)4Pd; LiCl / dioxane / 85 °C

3.1: Fe; glacial AcOH / 80 °C

4.1: 56 percent / NaHB(OAc)3; AcOH / tetrahydrofuran; CH₂Cl₂ / 20 °C

5.1: 100 percent / aq. NaOH / methanol / 65 °C

6.1: 1-hydroxybenzotriazole; PS-carbodiimide / CH₂Cl₂; dimethylformamide / 0.25 h

6.2: 0.52 g / N-methylmorpholine / CH₂Cl₂; dimethylformamide

With sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; PS-carbodiimide; sodium tris(acetoxy)borohydride; iron; benzotriazol-1-ol; acetic acid; triethylamine; lithium chloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; 2.1: Stille coupling;
DOI:10.1021/jm030233b

Reference yield:

: 361337-03-3
methyl (4-amino-3-methoxy-1,1'-biphenyl-2-yl)acetate

: 361337-06-6
benzyl imino(4-{[({3-methoxy-4-[(2-phenylethyl)amino]-1,1'-biphenyl-2-yl}acetyl)amino]methyl}phenyl)methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 56 percent / NaHB(OAc)3; AcOH / tetrahydrofuran; CH₂Cl₂ / 20 °C

2.1: 100 percent / aq. NaOH / methanol / 65 °C

3.1: 1-hydroxybenzotriazole; PS-carbodiimide / CH₂Cl₂; dimethylformamide / 0.25 h

3.2: 0.52 g / N-methylmorpholine / CH₂Cl₂; dimethylformamide

With sodium hydroxide; PS-carbodiimide; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; acetic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm030233b

Reference yield:

: 361337-02-2
methyl (3-methoxy-4-nitro-1,1'-biphenyl-2-yl)acetate

: 361337-06-6
benzyl imino(4-{[({3-methoxy-4-[(2-phenylethyl)amino]-1,1'-biphenyl-2-yl}acetyl)amino]methyl}phenyl)methylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: Fe; glacial AcOH / 80 °C

2.1: 56 percent / NaHB(OAc)3; AcOH / tetrahydrofuran; CH₂Cl₂ / 20 °C

3.1: 100 percent / aq. NaOH / methanol / 65 °C

4.1: 1-hydroxybenzotriazole; PS-carbodiimide / CH₂Cl₂; dimethylformamide / 0.25 h

4.2: 0.52 g / N-methylmorpholine / CH₂Cl₂; dimethylformamide

With sodium hydroxide; PS-carbodiimide; sodium tris(acetoxy)borohydride; iron; benzotriazol-1-ol; acetic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm030233b