4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-5-(p-tolyl)-Δ²-1,2,4-oxadiazoline

Base Information

Chemical Name:4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-5-(p-tolyl)-Δ²-1,2,4-oxadiazoline
CAS No.:80650-31-3
Molecular Formula:C₂₇H₂₃N₃O₂
Molecular Weight:421.499
Hs Code.:

4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-5-(p-tolyl)-Δ<sup>2</sup>-1,2,4-oxadiazoline

Synonyms:4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-5-(p-tolyl)-Δ²-1,2,4-oxadiazoline

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Chemical Property of 4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-5-(p-tolyl)-Δ²-1,2,4-oxadiazoline

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Technology Process of 4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-5-(p-tolyl)-Δ²-1,2,4-oxadiazoline

There total 3 articles about 4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-5-(p-tolyl)-Δ²-1,2,4-oxadiazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 80650-24-4
4-(p-methylbenzalamino)-3-methyl-5-styrylisoxazole

: 698-16-8
benzohydroximoyl chloride

: 80650-31-3
4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-5-(p-tolyl)-Δ²-1,2,4-oxadiazoline

Guidance literature:: With triethylamine; In chloroform; at 0 ℃; for 4.25h;

Reference yield:

: 53558-01-3
4-amino-3-methyl-5-styryl isoxazole

: 80650-31-3
4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-5-(p-tolyl)-Δ²-1,2,4-oxadiazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / methanol / Heating

2: 70 percent / Et₃N / CHCl₃ / 4.25 h / 0 °C

With triethylamine; In methanol; chloroform;

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 80650-31-3
4-(3-methyl-5-styryl-4-isoxazolyl)-3-phenyl-5-(p-tolyl)-Δ²-1,2,4-oxadiazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / methanol / Heating

2: 70 percent / Et₃N / CHCl₃ / 4.25 h / 0 °C

With triethylamine; In methanol; chloroform;